Benzoic acid (3R,4R,5R,6S)-5-azido-6-((3R,4R,5R,6S)-5-azido-4-benzyloxy-6-methoxy-tetrahydro-pyran-3-yloxy)-4-hydroxy-tetrahydro-pyran-3-yl ester

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Chemical Name:Benzoic acid (3R,4R,5R,6S)-5-azido-6-((3R,4R,5R,6S)-5-azido-4-benzyloxy-6-methoxy-tetrahydro-pyran-3-yloxy)-4-hydroxy-tetrahydro-pyran-3-yl ester
CAS No.:109200-43-3
Molecular Formula:C₂₅H₂₈N₆O₈
Molecular Weight:540.533
Hs Code.:

Synonyms:Benzoic acid (3R,4R,5R,6S)-5-azido-6-((3R,4R,5R,6S)-5-azido-4-benzyloxy-6-methoxy-tetrahydro-pyran-3-yloxy)-4-hydroxy-tetrahydro-pyran-3-yl ester

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Chemical Property of Benzoic acid (3R,4R,5R,6S)-5-azido-6-((3R,4R,5R,6S)-5-azido-4-benzyloxy-6-methoxy-tetrahydro-pyran-3-yloxy)-4-hydroxy-tetrahydro-pyran-3-yl ester

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Technology Process of Benzoic acid (3R,4R,5R,6S)-5-azido-6-((3R,4R,5R,6S)-5-azido-4-benzyloxy-6-methoxy-tetrahydro-pyran-3-yloxy)-4-hydroxy-tetrahydro-pyran-3-yl ester

There total 12 articles about Benzoic acid (3R,4R,5R,6S)-5-azido-6-((3R,4R,5R,6S)-5-azido-4-benzyloxy-6-methoxy-tetrahydro-pyran-3-yloxy)-4-hydroxy-tetrahydro-pyran-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

: 109200-42-2
methyl 2-azido-4-O-(2-azido-2-deoxy-β-D-xylopyranosyl)-3-O-benzyl-2-deoxy-α-D-xylopyranoside

: 98-88-4
benzoyl chloride

: 109200-43-3
Benzoic acid (3R,4R,5R,6S)-5-azido-6-((3R,4R,5R,6S)-5-azido-4-benzyloxy-6-methoxy-tetrahydro-pyran-3-yloxy)-4-hydroxy-tetrahydro-pyran-3-yl ester

: Benzoic acid (2S,3R,4R,5R)-3-azido-2-((3R,4R,5R,6S)-5-azido-4-benzyloxy-6-methoxy-tetrahydro-pyran-3-yloxy)-5-hydroxy-tetrahydro-pyran-4-yl ester

: C₃₂H₃₂N₆O₉

Guidance literature:: With triethylamine; In acetone; for 18h; Ambient temperature;
DOI:10.1246/bcsj.59.3137

Reference yield:

: 83030-01-7
methyl 2-azido-3-O-benzyl-2-deoxy-α-D-xylopyranoside

: 109200-43-3
Benzoic acid (3R,4R,5R,6S)-5-azido-6-((3R,4R,5R,6S)-5-azido-4-benzyloxy-6-methoxy-tetrahydro-pyran-3-yloxy)-4-hydroxy-tetrahydro-pyran-3-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) silver perchlorate, 2,4,6-trimethylpyridine, Drierite / 1.) nitromethane, -10 degC, 1 h; 2.) nitromethane, -10 degC, 60 h

2: sodium methoxide / methanol

3: 61 percent / triethylamine / acetone / 18 h / Ambient temperature

With 2,4,6-trimethyl-pyridine; calcium sulfate; sodium methylate; silver perchlorate; triethylamine; In methanol; acetone;
DOI:10.1246/bcsj.59.3137

Reference yield:

: 83022-09-7
3,4-di-O-acetyl-2-azido-2-deoxy-α-D-xylopyranosyl chloride

: 109200-43-3
Benzoic acid (3R,4R,5R,6S)-5-azido-6-((3R,4R,5R,6S)-5-azido-4-benzyloxy-6-methoxy-tetrahydro-pyran-3-yloxy)-4-hydroxy-tetrahydro-pyran-3-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) silver perchlorate, 2,4,6-trimethylpyridine, Drierite / 1.) nitromethane, -10 degC, 1 h; 2.) nitromethane, -10 degC, 60 h

2: sodium methoxide / methanol

3: 61 percent / triethylamine / acetone / 18 h / Ambient temperature

With 2,4,6-trimethyl-pyridine; calcium sulfate; sodium methylate; silver perchlorate; triethylamine; In methanol; acetone;
DOI:10.1246/bcsj.59.3137