methyl 2-amino-4-O-(4-O-benzoyl-2,3-dideoxy-2,3-epimino-β-D-ribopyranosyl)-3-O-benzyl-α-D-xylopyranoside

Base Information

Chemical Name:methyl 2-amino-4-O-(4-O-benzoyl-2,3-dideoxy-2,3-epimino-β-D-ribopyranosyl)-3-O-benzyl-α-D-xylopyranoside
CAS No.:83022-20-2
Molecular Formula:C₂₅H₃₀N₂O₇
Molecular Weight:470.522
Hs Code.:

Synonyms:methyl 2-amino-4-O-(4-O-benzoyl-2,3-dideoxy-2,3-epimino-β-D-ribopyranosyl)-3-O-benzyl-α-D-xylopyranoside

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Chemical Property of methyl 2-amino-4-O-(4-O-benzoyl-2,3-dideoxy-2,3-epimino-β-D-ribopyranosyl)-3-O-benzyl-α-D-xylopyranoside

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Technology Process of methyl 2-amino-4-O-(4-O-benzoyl-2,3-dideoxy-2,3-epimino-β-D-ribopyranosyl)-3-O-benzyl-α-D-xylopyranoside

There total 14 articles about methyl 2-amino-4-O-(4-O-benzoyl-2,3-dideoxy-2,3-epimino-β-D-ribopyranosyl)-3-O-benzyl-α-D-xylopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 83030-03-9
Benzoic acid (3R,4R,5R,6S)-5-amino-6-((3R,4R,5R,6S)-5-amino-4-benzyloxy-6-methoxy-tetrahydro-pyran-3-yloxy)-4-methanesulfonyloxy-tetrahydro-pyran-3-yl ester

: 83022-20-2
methyl 2-amino-4-O-(4-O-benzoyl-2,3-dideoxy-2,3-epimino-β-D-ribopyranosyl)-3-O-benzyl-α-D-xylopyranoside

Guidance literature:: With sodium acetate; In N,N-dimethyl-formamide; at 80 ℃; for 3h;
DOI:10.1016/S0040-4039(00)87195-6

Reference yield:

: 83030-01-7
methyl 2-azido-3-O-benzyl-2-deoxy-α-D-xylopyranoside

: 83022-20-2
methyl 2-amino-4-O-(4-O-benzoyl-2,3-dideoxy-2,3-epimino-β-D-ribopyranosyl)-3-O-benzyl-α-D-xylopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) silver perchlorate, 2,4,6-trimethylpyridine, Drierite / 1.) nitromethane, -10 degC, 1 h; 2.) nitromethane, -10 degC, 60 h

2: sodium methoxide / methanol

3: 61 percent / triethylamine / acetone / 18 h / Ambient temperature

4: 97 percent / pyridine

5: hydrogen / platinum oxide / CH₂Cl₂

6: 90 percent / sodium acetate / dimethylformamide; H₂O / 3 h / 80 °C

With 2,4,6-trimethyl-pyridine; calcium sulfate; hydrogen; sodium methylate; sodium acetate; silver perchlorate; triethylamine; platinum(IV) oxide; In pyridine; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1246/bcsj.59.3137

Reference yield:

: 109200-43-3
Benzoic acid (3R,4R,5R,6S)-5-azido-6-((3R,4R,5R,6S)-5-azido-4-benzyloxy-6-methoxy-tetrahydro-pyran-3-yloxy)-4-hydroxy-tetrahydro-pyran-3-yl ester

: 83022-20-2
methyl 2-amino-4-O-(4-O-benzoyl-2,3-dideoxy-2,3-epimino-β-D-ribopyranosyl)-3-O-benzyl-α-D-xylopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / pyridine

2: hydrogen / platinum oxide / CH₂Cl₂

3: 90 percent / sodium acetate / dimethylformamide; H₂O / 3 h / 80 °C

With hydrogen; sodium acetate; platinum(IV) oxide; In pyridine; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.59.3137