4'-chloro-2-((4-methoxyphenyl)sulfinyl)-5-(trifluoromethyl)-1,1'-biphenyl

Base Information

Chemical Name:4'-chloro-2-((4-methoxyphenyl)sulfinyl)-5-(trifluoromethyl)-1,1'-biphenyl
CAS No.:1158986-98-1
Molecular Formula:C₂₀H₁₄ClF₃O₂S
Molecular Weight:410.844
Hs Code.:

Synonyms:4'-chloro-2-((4-methoxyphenyl)sulfinyl)-5-(trifluoromethyl)-1,1'-biphenyl

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Chemical Property of 4'-chloro-2-((4-methoxyphenyl)sulfinyl)-5-(trifluoromethyl)-1,1'-biphenyl

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Technology Process of 4'-chloro-2-((4-methoxyphenyl)sulfinyl)-5-(trifluoromethyl)-1,1'-biphenyl

There total 2 articles about 4'-chloro-2-((4-methoxyphenyl)sulfinyl)-5-(trifluoromethyl)-1,1'-biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 637-87-6
1-Chloro-4-iodobenzene

: 398126-90-4
1-methoxy-4-{[4-(trifluoromethyl)phenyl]sulfinyl}benzene

: 1158986-98-1
4'-chloro-2-((4-methoxyphenyl)sulfinyl)-5-(trifluoromethyl)-1,1'-biphenyl

Guidance literature:: 1-methoxy-4-{[4-(trifluoromethyl)phenyl]sulfinyl}benzene; With 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex; In tetrahydrofuran; at -30 ℃; Inert atmosphere;

With zinc(II) chloride; In tetrahydrofuran; at 25 ℃; Inert atmosphere;

1-Chloro-4-iodobenzene; With trifuran-2-yl-phosphane; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; at 50 ℃; for 7h; Inert atmosphere;
DOI:10.1002/chem.201003657

Reference yield:

: 31401-23-7
p-methoxybenzenesulfinyl chloride

: 1158986-98-1
4'-chloro-2-((4-methoxyphenyl)sulfinyl)-5-(trifluoromethyl)-1,1'-biphenyl

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / -20 - 25 °C / Inert atmosphere

2.1: 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex / tetrahydrofuran / -30 °C / Inert atmosphere

2.2: 25 °C / Inert atmosphere

2.3: 7 h / 50 °C / Inert atmosphere

With 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex; In tetrahydrofuran;
DOI:10.1002/chem.201003657