4-bromo-2-methoxy-3,5,6-trimethylpyridine

Base Information

Chemical Name:4-bromo-2-methoxy-3,5,6-trimethylpyridine
CAS No.:640721-53-5
Molecular Formula:C₉H₁₂BrNO
Molecular Weight:230.104
Hs Code.:
Mol file:640721-53-5.mol

Synonyms:4-bromo-2-methoxy-3,5,6-trimethylpyridine

Suppliers and Price of 4-bromo-2-methoxy-3,5,6-trimethylpyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Chemenu
4-bromo-2-methoxy-3,5,6-trimethylpyridine 95%
1g
$ 720.00

Alichem
4-Bromo-2-methoxy-3,5,6-trimethylpyridine
1g
$ 626.20

Total 3 raw suppliers

Chemical Property of 4-bromo-2-methoxy-3,5,6-trimethylpyridine

Chemical Property:

Storage Temp.:2-8°C

Purity/Quality:

95+% ^*data from raw suppliers

4-bromo-2-methoxy-3,5,6-trimethylpyridine 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-bromo-2-methoxy-3,5,6-trimethylpyridine

There total 2 articles about 4-bromo-2-methoxy-3,5,6-trimethylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 121767-78-0
4-bromo-3,5,6-trimethyl-2(1H)-pyridone

: 74-88-4
methyl iodide

: 640721-53-5
4-bromo-2-methoxy-3,5,6-trimethylpyridine

Guidance literature:: With silver carbonate; In benzene; at 45 ℃; for 12h;
DOI:10.1021/ol0357503 DOI:10.1016/j.tet.2006.04.074

Reference yield:

: 109371-16-6
4-hydroxy-3,5,6-trimethyl-2(1H)-pyridone

: 640721-53-5
4-bromo-2-methoxy-3,5,6-trimethylpyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / POBr₃ / 1 h / 110 °C

2: 100 percent / Ag₂CO₃ / benzene / 12 h / 45 °C

With silver carbonate; phosphorus(V) oxybromide; In benzene;
DOI:10.1021/ol0357503

Reference yield: 89.0%

: 2996-92-1,46143-12-8
phenyl trimethylsiloxane

: 640721-53-5
4-bromo-2-methoxy-3,5,6-trimethylpyridine

: 2-methoxy-3,5,6-trimethyl-4-phenylpyridine

Guidance literature:: With tetrabutyl ammonium fluoride; triphenylphosphine; palladium diacetate; In N,N-dimethyl-formamide; at 80 ℃; for 12h;
DOI:10.1021/ol0357503