methyl 3-{3,4-bis[3-(4-dodecyl-1-oxyphenyl)propyl-1-oxy]phenyl}propionate

Base Information

Chemical Name:methyl 3-{3,4-bis[3-(4-dodecyl-1-oxyphenyl)propyl-1-oxy]phenyl}propionate
CAS No.:883196-36-9
Molecular Formula:C₅₂H₈₀O₆
Molecular Weight:801.204
Hs Code.:

Synonyms:methyl 3-{3,4-bis[3-(4-dodecyl-1-oxyphenyl)propyl-1-oxy]phenyl}propionate

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Chemical Property of methyl 3-{3,4-bis[3-(4-dodecyl-1-oxyphenyl)propyl-1-oxy]phenyl}propionate

Chemical Property:

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Technology Process of methyl 3-{3,4-bis[3-(4-dodecyl-1-oxyphenyl)propyl-1-oxy]phenyl}propionate

There total 11 articles about methyl 3-{3,4-bis[3-(4-dodecyl-1-oxyphenyl)propyl-1-oxy]phenyl}propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 883196-27-8
3-(4-(dodecyl-1-oxy)phenyl)propyl bromide

: 3598-22-9
methyl 3-(3,4-dihydroxyphenyl)propionate

: 883196-36-9
methyl 3-{3,4-bis[3-(4-dodecyl-1-oxyphenyl)propyl-1-oxy]phenyl}propionate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 16h;
DOI:10.1021/ja060062a

Reference yield:

: 5597-50-2
3-(4-hydroxyphenyl)propionic acid methyl ester

: 883196-36-9
methyl 3-{3,4-bis[3-(4-dodecyl-1-oxyphenyl)propyl-1-oxy]phenyl}propionate

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / K₂CO₃ / dimethylformamide / 12 h / 80 °C

2: 96 percent / LiAlH₄ / tetrahydrofuran / 0.5 h / 0 °C

3: 91 percent / CBr₄; PPh₃ / CH₂Cl₂ / 2 h / 0 °C

4: 86 percent / K₂CO₃ / dimethylformamide / 16 h / 80 °C

With lithium aluminium tetrahydride; carbon tetrabromide; potassium carbonate; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja060062a

Reference yield:

: 99-50-3
3,4-Dihydroxybenzoic acid

: 883196-36-9
methyl 3-{3,4-bis[3-(4-dodecyl-1-oxyphenyl)propyl-1-oxy]phenyl}propionate

Guidance literature:: Multi-step reaction with 8 steps

1: H₂SO₄ / Heating

2: 86 percent / K₂CO₃ / dimethylformamide / 8 h / 75 °C

3: 94 percent / LiAlH₄ / tetrahydrofuran / 0 - 20 °C

4: pyridinium chlorochromate / CH₂Cl₂ / 20 °C

5: 90 percent / morpholine; AcOH / Heating

6: 95 percent / p-toluenesulfonic acid monohydrate / 24 h / Heating

7: 91 percent / H₂ / Pd/C / ethanol

8: 86 percent / K₂CO₃ / dimethylformamide / 16 h / 80 °C

With morpholine; lithium aluminium tetrahydride; sulfuric acid; hydrogen; potassium carbonate; toluene-4-sulfonic acid; acetic acid; pyridinium chlorochromate; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; 1: Fisher esterification / 5: Knoevenagel condensation;
DOI:10.1021/ja060062a