1-(2-bromo-4,5-dimethoxybenzyl)-2-ethoxycarbonyl-1,2,3,4-tetrahydro-7-hydroxy-6-methoxyisoquinoline

Base Information

Chemical Name:1-(2-bromo-4,5-dimethoxybenzyl)-2-ethoxycarbonyl-1,2,3,4-tetrahydro-7-hydroxy-6-methoxyisoquinoline
CAS No.:51015-09-9
Molecular Formula:C₂₂H₂₆BrNO₆
Molecular Weight:480.356
Hs Code.:

Synonyms:1-(2-bromo-4,5-dimethoxybenzyl)-2-ethoxycarbonyl-1,2,3,4-tetrahydro-7-hydroxy-6-methoxyisoquinoline

Suppliers and Price of 1-(2-bromo-4,5-dimethoxybenzyl)-2-ethoxycarbonyl-1,2,3,4-tetrahydro-7-hydroxy-6-methoxyisoquinoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-(2-bromo-4,5-dimethoxybenzyl)-2-ethoxycarbonyl-1,2,3,4-tetrahydro-7-hydroxy-6-methoxyisoquinoline

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(2-bromo-4,5-dimethoxybenzyl)-2-ethoxycarbonyl-1,2,3,4-tetrahydro-7-hydroxy-6-methoxyisoquinoline

There total 4 articles about 1-(2-bromo-4,5-dimethoxybenzyl)-2-ethoxycarbonyl-1,2,3,4-tetrahydro-7-hydroxy-6-methoxyisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.8%

: 123190-18-1
1-(2-bromo-4,5-dimethoxybenzyl)-2-ethoxycarbonyl-1,2,3,4-tetrahydro-7-ethoxycarbonyl-6-methoxyisoquinoline

: 51015-09-9
1-(2-bromo-4,5-dimethoxybenzyl)-2-ethoxycarbonyl-1,2,3,4-tetrahydro-7-hydroxy-6-methoxyisoquinoline

Guidance literature:: With sodium hydroxide; In ethanol; water; for 0.25h; Heating;

Reference yield:

: 47706-26-3
7-benzyloxy-1-(2-bromo-4,5-dimethoxybenzyl)-1,2,3,4-tetrahydro-6-methoxyisoquinoline

: 51015-09-9
1-(2-bromo-4,5-dimethoxybenzyl)-2-ethoxycarbonyl-1,2,3,4-tetrahydro-7-hydroxy-6-methoxyisoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: 93.5 percent / conc. HCl / ethanol / 3 h / Heating

2: 80.6 percent / Et₃N / CHCl₃ / 1.) 10 deg C, 0.5 h, 2.) room temperature, 0.5 h

3: 74.8 percent / NaOH / ethanol; H₂O / 0.25 h / Heating

With hydrogenchloride; sodium hydroxide; triethylamine; In ethanol; chloroform; water;

Reference yield:

: 120566-97-4
1-<2'-bromo-4',5'-dimethoxy>-7-hydroxy-6-methoxy-1,2,3,4-tetrahydroisoquinoline

: 51015-09-9
1-(2-bromo-4,5-dimethoxybenzyl)-2-ethoxycarbonyl-1,2,3,4-tetrahydro-7-hydroxy-6-methoxyisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 80.6 percent / Et₃N / CHCl₃ / 1.) 10 deg C, 0.5 h, 2.) room temperature, 0.5 h

2: 74.8 percent / NaOH / ethanol; H₂O / 0.25 h / Heating

With sodium hydroxide; triethylamine; In ethanol; chloroform; water;