5-chloropentanoic acid (4-{4-[(benzylmethylamino)methyl]benzoyl}phenyl)amide

Base Information

Chemical Name:5-chloropentanoic acid (4-{4-[(benzylmethylamino)methyl]benzoyl}phenyl)amide
CAS No.:1298055-73-8
Molecular Formula:C₂₇H₂₉ClN₂O₂
Molecular Weight:448.992
Hs Code.:

Synonyms:5-chloropentanoic acid (4-{4-[(benzylmethylamino)methyl]benzoyl}phenyl)amide

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Chemical Property of 5-chloropentanoic acid (4-{4-[(benzylmethylamino)methyl]benzoyl}phenyl)amide

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Technology Process of 5-chloropentanoic acid (4-{4-[(benzylmethylamino)methyl]benzoyl}phenyl)amide

There total 4 articles about 5-chloropentanoic acid (4-{4-[(benzylmethylamino)methyl]benzoyl}phenyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1575-61-7
5-Chlorovaleroyl chloride

: 1298055-71-6
(4-aminophenyl)(4-((benzyl(methyl)amino)methyl)phenyl)methanone

: 1298055-73-8
5-chloropentanoic acid (4-{4-[(benzylmethylamino)methyl]benzoyl}phenyl)amide

Guidance literature:: In acetonitrile; for 6h; Reflux;
DOI:10.1016/j.ejmech.2011.02.019

Reference yield:

: 1298055-70-5
(4-((benzyl(methyl)amino)methyl)phenyl)(4-nitrophenyl)methanone

: 1298055-73-8
5-chloropentanoic acid (4-{4-[(benzylmethylamino)methyl]benzoyl}phenyl)amide

Guidance literature:: Multi-step reaction with 2 steps

1: 10% Pd/CaCO3; hydrogen / tetrahydrofuran / 20 °C

2: acetonitrile / 6 h / Reflux

With 10% Pd/CaCO3; hydrogen; In tetrahydrofuran; acetonitrile;
DOI:10.1016/j.ejmech.2011.02.019

Reference yield:

: 120712-34-7
4-(4-bromomethylbenzoyl)-nitrobenzene

: 1298055-73-8
5-chloropentanoic acid (4-{4-[(benzylmethylamino)methyl]benzoyl}phenyl)amide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / toluene / 12 h / Reflux

2: 10% Pd/CaCO3; hydrogen / tetrahydrofuran / 20 °C

3: acetonitrile / 6 h / Reflux

With 10% Pd/CaCO3; hydrogen; triethylamine; In tetrahydrofuran; toluene; acetonitrile;
DOI:10.1016/j.ejmech.2011.02.019