allyl O-(3,4,6-tri-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranosyl)-(1->4)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

Base Information

Chemical Name:allyl O-(3,4,6-tri-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranosyl)-(1->4)-2,4,6-tri-O-benzyl-α-D-galactopyranoside
CAS No.:129437-65-6
Molecular Formula:C₄₄H₅₂ClNO₁₄
Molecular Weight:854.348
Hs Code.:

Synonyms:allyl O-(3,4,6-tri-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranosyl)-(1->4)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

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Chemical Property of allyl O-(3,4,6-tri-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranosyl)-(1->4)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

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Technology Process of allyl O-(3,4,6-tri-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranosyl)-(1->4)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

There total 5 articles about allyl O-(3,4,6-tri-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranosyl)-(1->4)-2,4,6-tri-O-benzyl-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 61893-74-1
allyl 2,3,6-tri-O-benzyl-α-D-galactopyranoside

: 68499-56-9
1,3,4,6-tetra-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranoside

: 129437-65-6
allyl O-(3,4,6-tri-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranosyl)-(1->4)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

Guidance literature:: With 3 A molecular sieve; iron(III) chloride; In dichloromethane; for 6h; Ambient temperature;
DOI:10.1016/0008-6215(90)84083-7

Reference yield:

: 5432-46-2,10034-19-2,10034-20-5,34948-62-4,110253-00-4,1191127-63-5
1,3,4,6-tetra-O-acetyl-D-glucosamine hydrochloride

: 129437-65-6
allyl O-(3,4,6-tri-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranosyl)-(1->4)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / triethylamine / CH₂Cl₂

2: 78 percent / FeCl₃, molecular sieves (3 Angstroem) / CH₂Cl₂ / 6 h / Ambient temperature

With 3 A molecular sieve; iron(III) chloride; triethylamine; In dichloromethane;
DOI:10.1016/0008-6215(90)84083-7

Reference yield:

: 100-39-0
benzyl bromide

: 129437-65-6
allyl O-(3,4,6-tri-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranosyl)-(1->4)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / NaH / dimethylformamide

2: 81 percent / NaBH₃CN

3: 78 percent / FeCl₃, molecular sieves (3 Angstroem) / CH₂Cl₂ / 6 h / Ambient temperature

With 3 A molecular sieve; iron(III) chloride; sodium hydride; sodium cyanoborohydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(90)84083-7