acrolein (R,R)-1,2-dicyclohexylethylene acetal

Base Information

Chemical Name:acrolein (R,R)-1,2-dicyclohexylethylene acetal
CAS No.:257861-22-6
Molecular Formula:C₁₇H₂₈O₂
Molecular Weight:264.408
Hs Code.:

Synonyms:acrolein (R,R)-1,2-dicyclohexylethylene acetal

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Chemical Property of acrolein (R,R)-1,2-dicyclohexylethylene acetal

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Technology Process of acrolein (R,R)-1,2-dicyclohexylethylene acetal

There total 1 articles about acrolein (R,R)-1,2-dicyclohexylethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 3054-95-3
acrylaldehyde diethyl acetal

: 120850-92-2
(1R,2R)-1,2-dicyclohexyl-1,2-ethanediol

: 257861-22-6
acrolein (R,R)-1,2-dicyclohexylethylene acetal

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/ja004140k

Reference yield: 84.0%

: 96-22-0
pentan-3-one

: 257861-22-6
acrolein (R,R)-1,2-dicyclohexylethylene acetal

: 6-(2-hydroxy-1,2-dicyclohexylethan-1-yl)oxy-3-ethylhex-5-en-3-ol

Guidance literature:: acrolein (R,R)-1,2-dicyclohexylethylene acetal; With titanium(IV) isopropylate; isopropylmagnesium chloride; In diethyl ether; at -50 - -40 ℃; for 1.5h;

pentan-3-one; In diethyl ether; at -40 - 20 ℃; Further stages.;
DOI:10.1021/ja004140k

Reference yield: 70.0%

: 22483-21-2
E-2-methylpropanal N-benzylimine

: 257861-22-6
acrolein (R,R)-1,2-dicyclohexylethylene acetal

: 257861-34-0
(E)-(4S)-4-(N-benzyl)amino-1-[(1R,2R)-2-hydroxy-1,2-dicyclohexylethyl]oxy-5-methyl-1-hexene

: (Z)-4-(N-benzyl)amino-1-[(1R,2R)-2-hydroxy-1,2-dicyclohexylethyl]oxy-5-methyl-1-hexene

Guidance literature:: acrolein (R,R)-1,2-dicyclohexylethylene acetal; With titanium(IV) isopropylate; isopropylmagnesium chloride; In diethyl ether; at -50 - -40 ℃; for 1.5h;

E-2-methylpropanal N-benzylimine; In diethyl ether; at -40 - 20 ℃; for 4h;
DOI:10.1021/ja004140k