1-(4-methoxyphenyl)-4-piperidinone oxime

Base Information

Chemical Name:1-(4-methoxyphenyl)-4-piperidinone oxime
CAS No.:259663-87-1
Molecular Formula:C₁₂H₁₆N₂O₂
Molecular Weight:220.271
Hs Code.:

Synonyms:1-(4-methoxyphenyl)-4-piperidinone oxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-methoxyphenyl)-4-piperidinone oxime

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Technology Process of 1-(4-methoxyphenyl)-4-piperidinone oxime

There total 2 articles about 1-(4-methoxyphenyl)-4-piperidinone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 94635-24-2
1-(4-methoxyphenyl)piperidin-4-one

: 259663-87-1
1-(4-methoxyphenyl)-4-piperidinone oxime

Guidance literature:: With hydroxylamine hydrochloride; potassium carbonate; In ethanol; water; Heating;
DOI:10.1021/ja983716r

Reference yield:

: 3592-25-4
1,5-dichloropentan-3-one

: 259663-87-1
1-(4-methoxyphenyl)-4-piperidinone oxime

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / methanol / 3 h / Heating

2: 84 percent / HCl salt of hydroxylamine; potassium carbonate / ethanol; H₂O / Heating

With hydroxylamine hydrochloride; sodium carbonate; potassium carbonate; In methanol; ethanol; water; 1: Condensation / 2: Addition;
DOI:10.1021/ja983716r