(E)-3-[5-(1,2-dimethyl-2-propenyl)-4-hydroxy-3-methoxyphenyl]-1-(4-hydroxyphenyl)-2-propen-1-one

Base Information

Chemical Name:(E)-3-[5-(1,2-dimethyl-2-propenyl)-4-hydroxy-3-methoxyphenyl]-1-(4-hydroxyphenyl)-2-propen-1-one
CAS No.:1412939-10-6
Molecular Formula:C₂₁H₂₂O₄
Molecular Weight:338.403
Hs Code.:

Synonyms:(E)-3-[5-(1,2-dimethyl-2-propenyl)-4-hydroxy-3-methoxyphenyl]-1-(4-hydroxyphenyl)-2-propen-1-one

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Chemical Property of (E)-3-[5-(1,2-dimethyl-2-propenyl)-4-hydroxy-3-methoxyphenyl]-1-(4-hydroxyphenyl)-2-propen-1-one

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Technology Process of (E)-3-[5-(1,2-dimethyl-2-propenyl)-4-hydroxy-3-methoxyphenyl]-1-(4-hydroxyphenyl)-2-propen-1-one

There total 3 articles about (E)-3-[5-(1,2-dimethyl-2-propenyl)-4-hydroxy-3-methoxyphenyl]-1-(4-hydroxyphenyl)-2-propen-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1412939-06-0
C₁₃H₁₆O₃

: 99-93-4
4-Hydroxyacetophenone

: 1412939-10-6
(E)-3-[5-(1,2-dimethyl-2-propenyl)-4-hydroxy-3-methoxyphenyl]-1-(4-hydroxyphenyl)-2-propen-1-one

Guidance literature:: With hydrogenchloride; In ethanol; at 0 - 5 ℃; for 2h; Cooling with ice;
DOI:10.1007/s00044-012-0282-9

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 1412939-10-6
(E)-3-[5-(1,2-dimethyl-2-propenyl)-4-hydroxy-3-methoxyphenyl]-1-(4-hydroxyphenyl)-2-propen-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 20 °C

2: N,N-dimethyl-aniline / 26 h / 185 °C / Inert atmosphere; Sealed tube

3: hydrogenchloride / ethanol / 2 h / 0 - 5 °C / Cooling with ice

With hydrogenchloride; potassium carbonate; N,N-dimethyl-aniline; In ethanol; acetone; 2: |Claisen Rearrangement / 3: |Claisen-Schmidt Condensation;
DOI:10.1007/s00044-012-0282-9

Reference yield:

: 39953-41-8
3-methoxy-4-[(3-methylbut-2-en-1-yl)oxy] benzaldehyde

: 1412939-10-6
(E)-3-[5-(1,2-dimethyl-2-propenyl)-4-hydroxy-3-methoxyphenyl]-1-(4-hydroxyphenyl)-2-propen-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-aniline / 26 h / 185 °C / Inert atmosphere; Sealed tube

2: hydrogenchloride / ethanol / 2 h / 0 - 5 °C / Cooling with ice

With hydrogenchloride; N,N-dimethyl-aniline; In ethanol; 1: |Claisen Rearrangement / 2: |Claisen-Schmidt Condensation;
DOI:10.1007/s00044-012-0282-9