C₂₂H₃₆O₃SSi

Base Information

Chemical Name:C₂₂H₃₆O₃SSi
CAS No.:1610029-88-3
Molecular Formula:C₂₂H₃₆O₃SSi
Molecular Weight:408.678
Hs Code.:

C<sub>22</sub>H<sub>36</sub>O<sub>3</sub>SSi

Synonyms:C₂₂H₃₆O₃SSi

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Chemical Property of C₂₂H₃₆O₃SSi

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Technology Process of C₂₂H₃₆O₃SSi

There total 8 articles about C₂₂H₃₆O₃SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1610030-10-8
C₁₆H₃₂O₄Si

: 882-33-7
diphenyldisulfane

: 1610029-88-3
C₂₂H₃₆O₃SSi

Guidance literature:: With pyridine; tributylphosphine; at 20 - 50 ℃; for 6.5h; Inert atmosphere;
DOI:10.1021/ol5006856

Reference yield:

: {(2R,3R)-3-[(R)-2-(4-Methoxy-benzyloxy)-1-methyl-ethyl]-oxiranyl}-methanol

: 1610029-88-3
C₂₂H₃₆O₃SSi

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium bis(2-methoxyethoxy)aluminium dihydride / dichloromethane; toluene / 22 h / 0 - 20 °C / Inert atmosphere

1.2: 1 h / 20 °C

2.1: pyridine / dichloromethane / 17 h / 0 - 20 °C / Inert atmosphere

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 2 h / 20 °C

4.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 2 h / 20 °C / Inert atmosphere

5.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / tetrahydrofuran / 168 h / 20 °C

6.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 1.5 h / -72 °C / Inert atmosphere

7.1: titanium(IV) isopropylate; diethyl (2R,3R)-tartrate / dichloromethane / 0.75 h / -30 °C / Molecular sieve; Inert atmosphere

7.2: 15 h / -30 °C / Molecular sieve; Inert atmosphere

8.1: pyridine; tributylphosphine / 6.5 h / 20 - 50 °C / Inert atmosphere

With pyridine; titanium(IV) isopropylate; diethyl (2R,3R)-tartrate; tributylphosphine; diisobutylaluminium hydride; sodium bis(2-methoxyethoxy)aluminium dihydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; hexane; dichloromethane; water; dimethyl sulfoxide; toluene; 5.1: |Wittig Olefination / 7.1: |Sharpless Asymmetric Epoxidation / 7.2: |Sharpless Asymmetric Epoxidation;
DOI:10.1021/ol5006856

Reference yield:

: 1453868-10-4
(3S,4R)-5-((4-methoxybenzyl)oxy)-4-methylpentane-1,3-diol

: 1610029-88-3
C₂₂H₃₆O₃SSi

Guidance literature:: Multi-step reaction with 7 steps

1.1: pyridine / dichloromethane / 17 h / 0 - 20 °C / Inert atmosphere

2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 2 h / 20 °C

3.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 2 h / 20 °C / Inert atmosphere

4.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / tetrahydrofuran / 168 h / 20 °C

5.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 1.5 h / -72 °C / Inert atmosphere

6.1: titanium(IV) isopropylate; diethyl (2R,3R)-tartrate / dichloromethane / 0.75 h / -30 °C / Molecular sieve; Inert atmosphere

6.2: 15 h / -30 °C / Molecular sieve; Inert atmosphere

7.1: pyridine; tributylphosphine / 6.5 h / 20 - 50 °C / Inert atmosphere

With pyridine; titanium(IV) isopropylate; diethyl (2R,3R)-tartrate; tributylphosphine; diisobutylaluminium hydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; hexane; dichloromethane; water; dimethyl sulfoxide; 4.1: |Wittig Olefination / 6.1: |Sharpless Asymmetric Epoxidation / 6.2: |Sharpless Asymmetric Epoxidation;
DOI:10.1021/ol5006856