methyl 4-(((2-((trans-4-(tert-butyl)cyclohexyl)oxy)-4-methylnaphthalen-1-yl)methyl)amino)bicyclo[2.2.2]octane-1-carboxylate

Base Information

Chemical Name:methyl 4-(((2-((trans-4-(tert-butyl)cyclohexyl)oxy)-4-methylnaphthalen-1-yl)methyl)amino)bicyclo[2.2.2]octane-1-carboxylate
CAS No.:1621064-79-6
Molecular Formula:C₃₂H₄₅NO₃
Molecular Weight:491.714
Hs Code.:

Synonyms:methyl 4-(((2-((trans-4-(tert-butyl)cyclohexyl)oxy)-4-methylnaphthalen-1-yl)methyl)amino)bicyclo[2.2.2]octane-1-carboxylate

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Chemical Property of methyl 4-(((2-((trans-4-(tert-butyl)cyclohexyl)oxy)-4-methylnaphthalen-1-yl)methyl)amino)bicyclo[2.2.2]octane-1-carboxylate

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Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of methyl 4-(((2-((trans-4-(tert-butyl)cyclohexyl)oxy)-4-methylnaphthalen-1-yl)methyl)amino)bicyclo[2.2.2]octane-1-carboxylate

There total 3 articles about methyl 4-(((2-((trans-4-(tert-butyl)cyclohexyl)oxy)-4-methylnaphthalen-1-yl)methyl)amino)bicyclo[2.2.2]octane-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 135908-33-7
methyl 4-aminobicyclo[2.2.2]octane-1-carboxylate hydrochloride

: 2-(cis-4-tert-butylcyclohexyloxy)-4-methyl-1-naphthaldehyde

: 1621064-79-6
methyl 4-(((2-((trans-4-(tert-butyl)cyclohexyl)oxy)-4-methylnaphthalen-1-yl)methyl)amino)bicyclo[2.2.2]octane-1-carboxylate

Guidance literature:: methyl 4-aminobicyclo[2.2.2]octane-1-carboxylate hydrochloride; 2-(cis-4-tert-butylcyclohexyloxy)-4-methyl-1-naphthaldehyde; With magnesium sulfate; In toluene; for 48h; Reflux;

With sodium tris(acetoxy)borohydride; In tetrahydrofuran; for 24h; Reflux;

Reference yield:

: 18508-91-3
methanesulfonic acid 4-tert-butylcyclohexyl ester

: 1621064-79-6
methyl 4-(((2-((trans-4-(tert-butyl)cyclohexyl)oxy)-4-methylnaphthalen-1-yl)methyl)amino)bicyclo[2.2.2]octane-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: caesium carbonate / tert-butyl alcohol / 6 h / Reflux

2.1: magnesium sulfate / toluene / 48 h / Reflux

2.2: 24 h / Reflux

With magnesium sulfate; caesium carbonate; In toluene; tert-butyl alcohol;

Reference yield:

: 79325-54-5
2-Hydroxy-4-methyl-1-naphthaldehyde

: 1621064-79-6
methyl 4-(((2-((trans-4-(tert-butyl)cyclohexyl)oxy)-4-methylnaphthalen-1-yl)methyl)amino)bicyclo[2.2.2]octane-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: caesium carbonate / tert-butyl alcohol / 6 h / Reflux

2.1: magnesium sulfate / toluene / 48 h / Reflux

2.2: 24 h / Reflux

With magnesium sulfate; caesium carbonate; In toluene; tert-butyl alcohol;