N-{2-[2-chloro-2-(toluene-4-sulfinyl)ethyl]phenyl}-N-methylcarbamic acid tert-butyl ester

Base Information

Chemical Name:N-{2-[2-chloro-2-(toluene-4-sulfinyl)ethyl]phenyl}-N-methylcarbamic acid tert-butyl ester
CAS No.:1190208-71-9
Molecular Formula:C₂₁H₂₆ClNO₃S
Molecular Weight:407.961
Hs Code.:

Synonyms:N-{2-[2-chloro-2-(toluene-4-sulfinyl)ethyl]phenyl}-N-methylcarbamic acid tert-butyl ester

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Chemical Property of N-{2-[2-chloro-2-(toluene-4-sulfinyl)ethyl]phenyl}-N-methylcarbamic acid tert-butyl ester

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Technology Process of N-{2-[2-chloro-2-(toluene-4-sulfinyl)ethyl]phenyl}-N-methylcarbamic acid tert-butyl ester

There total 1 articles about N-{2-[2-chloro-2-(toluene-4-sulfinyl)ethyl]phenyl}-N-methylcarbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 240493-91-8
(2-bromomethyl-phenyl)-methyl-carbamic acid tert-butyl ester

: 24824-93-9
chloromethyl p-tolyl sulfoxide

: 1190208-71-9
N-{2-[2-chloro-2-(toluene-4-sulfinyl)ethyl]phenyl}-N-methylcarbamic acid tert-butyl ester

Guidance literature:: chloromethyl p-tolyl sulfoxide; With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.166667h; Inert atmosphere;

(2-bromomethyl-phenyl)-methyl-carbamic acid tert-butyl ester; In tetrahydrofuran; at -78 - 0 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tetasy.2009.06.024

Reference yield: 93.0%

: 1190208-71-9
N-{2-[2-chloro-2-(toluene-4-sulfinyl)ethyl]phenyl}-N-methylcarbamic acid tert-butyl ester

: N-{2-[2-chloro-2-(toluene-4-sulfinyl)ethyl]phenyl}-N-methylamine

Guidance literature:: N-{2-[2-chloro-2-(toluene-4-sulfinyl)ethyl]phenyl}-N-methylcarbamic acid tert-butyl ester; With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 3h;

With water; sodium hydroxide; In dichloromethane; optical yield given as %de;
DOI:10.1016/j.tetasy.2009.06.024