N-<2-(3,4-Dimethoxyphenyl)ethyl>-2,2-ethylendioxy-1-cyclohexancarboxamid

Base Information

• Chemical Name: N-<2-(3,4-Dimethoxyphenyl)ethyl>-2,2-ethylendioxy-1-cyclohexancarboxamid
• CAS No.: 78632-11-8
• Molecular Formula: C₁₉H₂₇NO₅
• Molecular Weight: 349.427
• Mol file: 78632-11-8.mol

Synonyms:N-<2-(3,4-Dimethoxyphenyl)ethyl>-2,2-ethylendioxy-1-cyclohexancarboxamid

Chemical Property of N-<2-(3,4-Dimethoxyphenyl)ethyl>-2,2-ethylendioxy-1-cyclohexancarboxamid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-<2-(3,4-Dimethoxyphenyl)ethyl>-2,2-ethylendioxy-1-cyclohexancarboxamid

There total 2 articles about N-<2-(3,4-Dimethoxyphenyl)ethyl>-2,2-ethylendioxy-1-cyclohexancarboxamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1,4-dioxaspiro[4.5]decane-6-carboxylic acid (4746-93-4) + 2-(3,4-dimethoxyphenyl)-ethylamine (120-20-7) → N-<2-(3,4-Dimethoxyphenyl)ethyl>-2,2-ethylendioxy-1-cyclohexancarboxamid (78632-11-8)

Guidance literature:

In xylene; Heating;

Reference yield:

ethyl 2-oxocyclohexane carboxylate (1655-07-8) → N-<2-(3,4-Dimethoxyphenyl)ethyl>-2,2-ethylendioxy-1-cyclohexancarboxamid (78632-11-8)

Guidance literature:

Multi-step reaction with 2 steps

2: 95 percent / xylene / Heating

In xylene;

Reference yield: 40.0%

N-<2-(3,4-Dimethoxyphenyl)ethyl>-2,2-ethylendioxy-1-cyclohexancarboxamid (78632-11-8) → 2-Oxo-cyclohexanecarboxylic acid [2-(3,4-dimethoxy-phenyl)-ethyl]-amide (78632-12-9)

Guidance literature:

With hydrogenchloride; In methanol; at 40 ℃; for 0.5h;

upstream raw materials:

1,4-dioxaspiro[4.5]decane-6-carboxylic acid

2-(3,4-dimethoxyphenyl)-ethylamine

ethyl 2-oxocyclohexane carboxylate

Downstream raw materials:

2-Oxo-cyclohexanecarboxylic acid [2-(3,4-dimethoxy-phenyl)-ethyl]-amide

N-<2-(3,4-Dimethoxyphenyl)ethyl>-2,3,6,7,8,9-hexahydro-5H-1,4-benzodioxepin-5-imin

1-<(2,2-Ethylendioxy)cyclohexyl>-3,4-dihydro-6,7-dimethoxyisochinolin

2-(3,4-Dihydro-6,7-dimethoxy-1-isochinolinyl)-1-cyclohexen-1-ol