C₁₅H₁₇ClO₄

Base Information

Chemical Name:C₁₅H₁₇ClO₄
CAS No.:1541198-22-4
Molecular Formula:C₁₅H₁₇ClO₄
Molecular Weight:296.751
Hs Code.:

C<sub>15</sub>H<sub>17</sub>ClO<sub>4</sub>

Synonyms:C₁₅H₁₇ClO₄

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Chemical Property of C₁₅H₁₇ClO₄

Chemical Property:

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Technology Process of C₁₅H₁₇ClO₄

There total 4 articles about C₁₅H₁₇ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 230642-94-1
2-(3-chloro-5-formylphenyl)-2-methylpropanenitrile

: 765-85-5
methyl cyclobutanecarboxylate

: 1541198-22-4
C₁₅H₁₇ClO₄

Guidance literature:: methyl cyclobutanecarboxylate; With n-butyllithium; N-cyclohexyl-cyclohexanamine; In hexane; toluene; at 0 - 25 ℃; for 0.25h; Inert atmosphere;

2-(3-chloro-5-formylphenyl)-2-methylpropanenitrile; With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; In hexane; toluene; for 1h; Inert atmosphere;

Reference yield:

: 3721-95-7
Cyclobutanecarboxylic acid

: 1541198-22-4
C₁₅H₁₇ClO₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid / 8 h / 70 °C

2.1: n-butyllithium; N-cyclohexyl-cyclohexanamine / hexane; toluene / 0.25 h / 0 - 25 °C / Inert atmosphere

2.2: 1 h / Inert atmosphere

With n-butyllithium; sulfuric acid; N-cyclohexyl-cyclohexanamine; In hexane; toluene;

Reference yield:

: 14862-52-3
1,3-dibromo-5-chlorobenzene

: 1541198-22-4
C₁₅H₁₇ClO₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / hexane; di-isopropyl ether / 0.5 h / -78 °C / Inert atmosphere

1.2: -78 °C / Inert atmosphere

2.1: toluene-4-sulfonic acid / toluene / 6 h / Reflux; Dean-Stark

3.1: n-butyllithium; N-cyclohexyl-cyclohexanamine / hexane; toluene / 0.25 h / 0 - 25 °C / Inert atmosphere

3.2: 1 h / Inert atmosphere

With n-butyllithium; toluene-4-sulfonic acid; N-cyclohexyl-cyclohexanamine; In hexane; di-isopropyl ether; toluene;