4,6-Di-tert-butyl-2-ethoxy-2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-2-methyl-1,3-dioxa-2λ⁵-phospha-indan

Base Information

• Chemical Name: 4,6-Di-tert-butyl-2-ethoxy-2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-2-methyl-1,3-dioxa-2λ⁵-phospha-indan
• CAS No.: 129896-67-9
• Molecular Formula: C₂₇H₄₇O₄P
• Molecular Weight: 466.642

Synonyms:4,6-Di-tert-butyl-2-ethoxy-2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-2-methyl-1,3-dioxa-2λ⁵-phospha-indan

Chemical Property of 4,6-Di-tert-butyl-2-ethoxy-2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-2-methyl-1,3-dioxa-2λ⁵-phospha-indan

Chemical Property:

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Technology Process of 4,6-Di-tert-butyl-2-ethoxy-2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-2-methyl-1,3-dioxa-2λ⁵-phospha-indan

There total 3 articles about 4,6-Di-tert-butyl-2-ethoxy-2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-2-methyl-1,3-dioxa-2λ⁵-phospha-indan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

ethanol (64-17-5) + [4,6-Di-tert-butyl-2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-2-methyl-1,3-dioxa-2λ5-phospha-indan-2-yl]-diisopropyl-amine → 4,6-Di-tert-butyl-2-ethoxy-2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-2-methyl-1,3-dioxa-2λ5-phospha-indan (129896-67-9)

Guidance literature:

In dichloromethane; at 25 ℃;

DOI:10.1021/ja00179a048

Reference yield:

(-)-menthol (2216-51-5) → 4,6-Di-tert-butyl-2-ethoxy-2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-2-methyl-1,3-dioxa-2λ5-phospha-indan (129896-67-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 88 percent / 1H-tetrazole / CH₂Cl₂ / 40 h / 25 °C

2: CH₂Cl₂ / 2 h / 0 °C

3: 94 percent / CH₂Cl₂ / 25 °C

With 1H-tetrazole; In dichloromethane;

DOI:10.1021/ja00179a048

Reference yield:

C17H36NOP (129896-64-6,129896-72-6) → 4,6-Di-tert-butyl-2-ethoxy-2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-2-methyl-1,3-dioxa-2λ5-phospha-indan (129896-67-9)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₂Cl₂ / 2 h / 0 °C

2: 94 percent / CH₂Cl₂ / 25 °C

In dichloromethane;

DOI:10.1021/ja00179a048

upstream raw materials:

ethanol

(-)-menthol

C₁₇H₃₆NOP

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