1-<3,5-bis-O-(p-chlorobenzoyl)-2-deoxy-β-D-ribofuranosyl>-5-bromo-2-pyrimidinone

Base Information

• Chemical Name: 1-<3,5-bis-O-(p-chlorobenzoyl)-2-deoxy-β-D-ribofuranosyl>-5-bromo-2-pyrimidinone
• CAS No.: 96245-83-9
• Molecular Formula: C₂₃H₁₇BrCl₂N₂O₆
• Molecular Weight: 568.208

Synonyms:1-<3,5-bis-O-(p-chlorobenzoyl)-2-deoxy-β-D-ribofuranosyl>-5-bromo-2-pyrimidinone

Chemical Property of 1-<3,5-bis-O-(p-chlorobenzoyl)-2-deoxy-β-D-ribofuranosyl>-5-bromo-2-pyrimidinone

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Technology Process of 1-<3,5-bis-O-(p-chlorobenzoyl)-2-deoxy-β-D-ribofuranosyl>-5-bromo-2-pyrimidinone

There total 1 articles about 1-<3,5-bis-O-(p-chlorobenzoyl)-2-deoxy-β-D-ribofuranosyl>-5-bromo-2-pyrimidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 7.7%

3,5-O-bis(4-chlorobenzoyl)-2-deoxy-α-D-ribofuranosyl chloride (21740-23-8) + 5-bromo-2-trimethylsilyloxypyrimidine (83768-01-8) → 1-<3,5-bis-O-(p-chlorobenzoyl)-2-deoxy-β-D-ribofuranosyl>-5-bromo-2-pyrimidinone (96245-83-9) + C23H17BrCl2N2O6 (96245-85-1)

Guidance literature:

With tin(IV) chloride; In dichloromethane; at 0 ℃;

DOI:10.1021/jm00145a010

Reference yield: 60.0%

1-<3,5-bis-O-(p-chlorobenzoyl)-2-deoxy-β-D-ribofuranosyl>-5-bromo-2-pyrimidinone (96245-83-9) → 1-(2-deoxy-β-D-ribofuranosyl)-5-bromo-2-pyrimidinone (96245-87-3)

Guidance literature:

With ammonia; In methanol; at 4 ℃; for 5h;

DOI:10.1021/jm00145a010

upstream raw materials:

3,5-O-bis(4-chlorobenzoyl)-2-deoxy-α-D-ribofuranosyl chloride

5-bromo-2-trimethylsilyloxypyrimidine

Downstream raw materials:

1-(2-deoxy-β-D-ribofuranosyl)-5-bromo-2-pyrimidinone

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