Technology Process of (9-hexyl-9H-carbazol-3-yl)(phenyl)methanone
There total 6 articles about (9-hexyl-9H-carbazol-3-yl)(phenyl)methanone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
aluminum (III) chloride;
In
dichloromethane;
DOI:10.1039/c4tc00097h
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium hydroxide; tetrabutylammomium bromide / water; benzene
2: aluminum (III) chloride / dichloromethane
With
aluminum (III) chloride; tetrabutylammomium bromide; potassium hydroxide;
In
dichloromethane; water; benzene;
2: |Friedel-Crafts Acylation;
DOI:10.1039/c4tc00097h
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: tetrakis(triphenylphosphine) palladium(0); potassium phosphate / ethanol / 12 h / 90 °C / Inert atmosphere
2.1: palladium diacetate; acetic acid; dihydrogen peroxide / 0.33 h / 120 °C / Inert atmosphere; Microwave irradiation; Sealed tube
3.1: tetrabutylammomium bromide; potassium hydroxide / N,N-dimethyl-formamide / 24 h / 70 °C / Inert atmosphere
4.1: aluminum (III) chloride / dichloromethane / 0.5 h / 0 °C / Inert atmosphere
4.2: 24.25 h / 0 - 30 °C / Inert atmosphere
With
aluminum (III) chloride; potassium phosphate; tetrakis(triphenylphosphine) palladium(0); tetrabutylammomium bromide; dihydrogen peroxide; palladium diacetate; acetic acid; potassium hydroxide;
In
ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.202005105
