tert-butyl 4-{2-[(2,4-dimethoxybenzyl)amino]-1-hydroxyethyl}piperidine-1-carboxylate

Base Information

Chemical Name:tert-butyl 4-{2-[(2,4-dimethoxybenzyl)amino]-1-hydroxyethyl}piperidine-1-carboxylate
CAS No.:1429500-82-2
Molecular Formula:C₂₁H₃₄N₂O₅
Molecular Weight:394.511
Hs Code.:

Synonyms:tert-butyl 4-{2-[(2,4-dimethoxybenzyl)amino]-1-hydroxyethyl}piperidine-1-carboxylate

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Chemical Property of tert-butyl 4-{2-[(2,4-dimethoxybenzyl)amino]-1-hydroxyethyl}piperidine-1-carboxylate

Chemical Property:

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Technology Process of tert-butyl 4-{2-[(2,4-dimethoxybenzyl)amino]-1-hydroxyethyl}piperidine-1-carboxylate

There total 3 articles about tert-butyl 4-{2-[(2,4-dimethoxybenzyl)amino]-1-hydroxyethyl}piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 613-45-6
2,4-Dimethoxybenzaldehyde

: 301221-57-8
tert-butyl 4-(2-amino-1-hydroxyethyl)piperidine-1-carboxylate?

: 1429500-82-2
tert-butyl 4-{2-[(2,4-dimethoxybenzyl)amino]-1-hydroxyethyl}piperidine-1-carboxylate

Guidance literature:: 2,4-Dimethoxybenzaldehyde; tert-butyl 4-(2-amino-1-hydroxyethyl)piperidine-1-carboxylate?; With acetic acid; In tetrahydrofuran; at 20 ℃; for 1h;

With sodium cyanoborohydride; In tetrahydrofuran; at 20 ℃; for 1h;

Reference yield:

: 137076-22-3
tert butyl 4-formylpiperidine-1-carboxylate

: 1429500-82-2
tert-butyl 4-{2-[(2,4-dimethoxybenzyl)amino]-1-hydroxyethyl}piperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran; nitromethane; tert-butyl alcohol

3: acetic acid; sodium cyanoborohydride / tetrahydrofuran

With sodium cyanoborohydride; acetic acid; In tetrahydrofuran; nitromethane; tert-butyl alcohol;

Reference yield:

: 301221-56-7
tert-butyl 4-(1-hydroxy-2-nitroethyl)piperidine-1-carboxylate

: 1429500-82-2
tert-butyl 4-{2-[(2,4-dimethoxybenzyl)amino]-1-hydroxyethyl}piperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

2: acetic acid; sodium cyanoborohydride / tetrahydrofuran

With sodium cyanoborohydride; acetic acid; In tetrahydrofuran;