3-Phenoxy-α-(diethoxyphosphinyl)benzenebutanesulfonic acid, cyclohexyl ester

Base Information

Chemical Name:3-Phenoxy-α-(diethoxyphosphinyl)benzenebutanesulfonic acid, cyclohexyl ester
CAS No.:157126-73-3
Molecular Formula:C₂₆H₃₇O₇PS
Molecular Weight:524.615
Hs Code.:

Synonyms:3-Phenoxy-α-(diethoxyphosphinyl)benzenebutanesulfonic acid, cyclohexyl ester

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Chemical Property of 3-Phenoxy-α-(diethoxyphosphinyl)benzenebutanesulfonic acid, cyclohexyl ester

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Technology Process of 3-Phenoxy-α-(diethoxyphosphinyl)benzenebutanesulfonic acid, cyclohexyl ester

There total 4 articles about 3-Phenoxy-α-(diethoxyphosphinyl)benzenebutanesulfonic acid, cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 60-29-7,927820-24-4
diethyl ether

: 157126-72-2
1-(3-iodopropyl)-3-phenoxybenzene

: 157126-73-3
3-Phenoxy-α-(diethoxyphosphinyl)benzenebutanesulfonic acid, cyclohexyl ester

Guidance literature:: In hexane; N,N-dimethyl-formamide;

Reference yield:

: cyclohexyl (diethyl methylphosphono)sulfonate

: 157126-72-2
1-(3-iodopropyl)-3-phenoxybenzene

: 157126-73-3
3-Phenoxy-α-(diethoxyphosphinyl)benzenebutanesulfonic acid, cyclohexyl ester

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 3h;
DOI:10.1021/jm801023u

Reference yield:

: 39515-51-0
3-Phenoxybenzaldehyde

: 157126-73-3
3-Phenoxy-α-(diethoxyphosphinyl)benzenebutanesulfonic acid, cyclohexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 - 20 °C

2.1: triethylamine; methanesulfonyl chloride / dichloromethane / 1 h / 0 °C

2.2: 1 h / 60 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 3 h / 0 - 20 °C

With sodium hydride; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil;