N-(2-Chlorophenyl)benzenecarbohydrazonoylchloride

Base Information

• Chemical Name: N-(2-Chlorophenyl)benzenecarbohydrazonoylchloride
• CAS No.: 26946-54-3
• Molecular Formula: C13H10 Cl2 N2
• Molecular Weight: 265.142
• Hs Code.: 2928000090
• Mol file: 26946-54-3.mol

Synonyms:Benzoylchloride, (o-chlorophenyl)hydrazone (7CI,8CI)

Chemical Property of N-(2-Chlorophenyl)benzenecarbohydrazonoylchloride

Chemical Property:

• Vapor Pressure: 1.42E-05mmHg at 25°C
• Refractive Index: 1.598
• Boiling Point: 366.9°C at 760 mmHg
• Flash Point: 175.7°C
• PSA: 24.39000
• Density: 1.24g/cm³
• LogP: 4.42550

Purity/Quality:

97% ^*data from raw suppliers

N-(2-Chlorophenyl)benzenecarbohydrazonoylchloride 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(2-Chlorophenyl)benzenecarbohydrazonoylchloride

There total 7 articles about N-(2-Chlorophenyl)benzenecarbohydrazonoylchloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

1-benzylidene-2-(2-chlorophenyl)hydrazine (2989-40-4) → N'-(2-chlorophenyl)benzohydrazonoyl chloride (26946-54-3)

Guidance literature:

With N-chloro-succinimide; dimethylsulfide; In dichloromethane; at -78 ℃; for 1h;

DOI:10.1016/j.ejmech.2017.09.037

Reference yield:

benzaldehyde (100-52-7) → N'-(2-chlorophenyl)benzohydrazonoyl chloride (26946-54-3)

Guidance literature:

Multi-step reaction with 2 steps

1: water; ethanol / 20 °C / Darkness

2: N-chloro-succinimide; dimethylsulfide / dichloromethane / 1 h / -78 °C

With N-chloro-succinimide; dimethylsulfide; In ethanol; dichloromethane; water;

DOI:10.1016/j.ejmech.2017.09.037

Reference yield:

(2-chlorophenyl)hydrazine (10449-07-7) → N'-(2-chlorophenyl)benzohydrazonoyl chloride (26946-54-3)

Guidance literature:

Multi-step reaction with 2 steps

1: water; ethanol / 20 °C / Darkness

2: N-chloro-succinimide; dimethylsulfide / dichloromethane / 1 h / -78 °C

With N-chloro-succinimide; dimethylsulfide; In ethanol; dichloromethane; water;

DOI:10.1016/j.ejmech.2017.09.037

upstream raw materials:

benzaldehyde

(2-chlorophenyl)hydrazine

1-benzylidene-2-(2-chlorophenyl)hydrazine

o-chlorophenylhydrazine hydrochloride

Downstream raw materials:

Bis-<α-(o-chlorphenylhydrazono)-benzyl>-sulfid

C₁₄H₉Cl₂N₃O₃S

ethyl 1-(2-chlorophenyl)-3,4-diphenyl-1H-pyrazole-5-carboxylate