1-(NH(2,6-i-Pr₂-C₆H₃))-2-(PPh₂=N(2,4,6-Me₃C₆H₂))C₆H₄

Base Information

Chemical Name:1-(NH(2,6-i-Pr₂-C₆H₃))-2-(PPh₂=N(2,4,6-Me₃C₆H₂))C₆H₄
CAS No.:676245-91-3
Molecular Formula:C₃₉H₄₃N₂P
Molecular Weight:570.758
Hs Code.:

1-(NH(2,6-i-Pr<sub>2</sub>-C<sub>6</sub>H<sub>3</sub>))-2-(PPh<sub>2</sub>=N(2,4,6-Me<sub>3</sub>C<sub>6</sub>H<sub>2</sub>))C<sub>6</sub>H<sub>4</sub>

Synonyms:1-(NH(2,6-i-Pr₂-C₆H₃))-2-(PPh₂=N(2,4,6-Me₃C₆H₂))C₆H₄

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Chemical Property of 1-(NH(2,6-i-Pr₂-C₆H₃))-2-(PPh₂=N(2,4,6-Me₃C₆H₂))C₆H₄

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Technology Process of 1-(NH(2,6-i-Pr₂-C₆H₃))-2-(PPh₂=N(2,4,6-Me₃C₆H₂))C₆H₄

There total 1 articles about 1-(NH(2,6-i-Pr₂-C₆H₃))-2-(PPh₂=N(2,4,6-Me₃C₆H₂))C₆H₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 599205-16-0
N-[2-(diphenylphosphino)phenyl]-2,6-diisopropylaniline

: 14213-00-4
2,4,6-trimethylaniline azide

: 676245-91-3
1-(NH(2,6-i-Pr₂-C₆H₃))-2-(PPh₂=N(2,4,6-Me₃C₆H₂))C₆H₄

Guidance literature:: In toluene; at 80 ℃; Inert atmosphere;
DOI:10.1002/ejic.201001362

Reference yield: 77.0%

: 676245-91-3
1-(NH(2,6-i-Pr₂-C₆H₃))-2-(PPh₂=N(2,4,6-Me₃C₆H₂))C₆H₄

: 544-97-8
dimethyl zinc(II)

: 1315607-94-3
(CH(CH₃)2)2C₆H₃NC₆H₄P(C₆H₅)2NC₆H₂(CH₃)3ZnCH₃

Guidance literature:: In diethyl ether; toluene; (N2), solid ligand dissolved in Et2O, cooled to -35°C, treated with 1 equiv. of ZnMe2 in toluene, warmed to room temp., stirred for 7 h; evapd., triturated (pentane), dissolved in Et2O, cooled to -35°C,crystd., elem. anal.;
DOI:10.1002/ejic.201001362

Reference yield: 75.0%

: 676245-91-3
1-(NH(2,6-i-Pr₂-C₆H₃))-2-(PPh₂=N(2,4,6-Me₃C₆H₂))C₆H₄

: 75-24-1
trimethylaluminum

: 676245-94-6
Al(CH₃)2[1-(N(2,6-i-Pr₂-C₆H₃))-2-(PPh₂=N(2,4,6-Me₃C₆H₂))C₆H₄]

Guidance literature:: In toluene; byproducts: CH4; to a soln. of phosphinimide in toluene was added a toluene soln. of Al(CH3)3 at -23°C, the soln. was stirred for 4 h at 50°C (Ar); evapd. to dryness in vac., the residue was slurried with isopentane, filtered at 23°C, the solid was dried in vac.; elem. anal.;
DOI:10.1021/om034302w