4-Phenylbut-2-enoic acid

Base Information

Chemical Name:4-Phenylbut-2-enoic acid
CAS No.:2243-52-9
Molecular Formula:C10H10 O2
Molecular Weight:162.188
Hs Code.:
DSSTox Substance ID:DTXSID50945114
Mol file:2243-52-9.mol

Synonyms:4-phenylbut-2-enoic acid;2243-52-9;4-Phenyl-2-butenoic acid;(E)-4-PHENYL-BUT-2-ENOIC ACID;DTXSID50945114;SCBUQIQXUBOQAI-UHFFFAOYSA-N

Suppliers and Price of 4-Phenylbut-2-enoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(E)-4-PHENYL-BUT-2-ENOIC ACID 95.00%
2G
$ 1443.75

Total 5 raw suppliers

Chemical Property of 4-Phenylbut-2-enoic acid

Chemical Property:

PSA：37.30000
LogP:1.86990
XLogP3:2.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:162.068079557
Heavy Atom Count:12
Complexity:167

Purity/Quality:

99% ^*data from raw suppliers

(E)-4-PHENYL-BUT-2-ENOIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)CC=CC(=O)O

Technology Process of 4-Phenylbut-2-enoic acid

There total 21 articles about 4-Phenylbut-2-enoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 4071-85-6
trimetylsilylketene

: 122-78-1
phenylacetaldehyde

: 2243-52-9
3-benzylacrylic acid

Guidance literature:: With boron trifluoride diethyl etherate; In diethyl ether; Ambient temperature;
DOI:10.1080/00397919508010783

Reference yield: 56.0%

: 141-82-2
malonic acid

: 122-78-1
phenylacetaldehyde

: 2243-52-9
3-benzylacrylic acid

Guidance literature:: malonic acid; phenylacetaldehyde; With piperidine; pyridine; for 2h; Reflux;

With hydrogenchloride; In water;
DOI:10.1016/j.ejmech.2012.09.021

Reference yield:

: 141-82-2
malonic acid

: 122-78-1
phenylacetaldehyde

: 2243-52-9
3-benzylacrylic acid

: 2243-53-0,59744-46-6,1914-58-5
trans-styrylacetic acid

Guidance literature:: malonic acid; phenylacetaldehyde; With 4-methyl-morpholine; at 80 ℃; for 8h;

With sulfuric acid; In water; at 20 ℃; for 0.5h; regioselective reaction;
DOI:10.1080/00397910903370659