3-tert-butyldimethylsilanyloxy-3-cyclohexyl-1-methylpropyl methanesulfonate

Base Information

Chemical Name:3-tert-butyldimethylsilanyloxy-3-cyclohexyl-1-methylpropyl methanesulfonate
CAS No.:497069-73-5
Molecular Formula:C₁₇H₃₆O₄SSi
Molecular Weight:364.622
Hs Code.:

Synonyms:3-tert-butyldimethylsilanyloxy-3-cyclohexyl-1-methylpropyl methanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-tert-butyldimethylsilanyloxy-3-cyclohexyl-1-methylpropyl methanesulfonate

Chemical Property:

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Technology Process of 3-tert-butyldimethylsilanyloxy-3-cyclohexyl-1-methylpropyl methanesulfonate

There total 4 articles about 3-tert-butyldimethylsilanyloxy-3-cyclohexyl-1-methylpropyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 497069-74-6
4-tertbutyldimethylsilanyloxy-4-cyclohexyl-2-butanol

: 124-63-0
methanesulfonyl chloride

: 497069-73-5
3-tert-butyldimethylsilanyloxy-3-cyclohexyl-1-methylpropyl methanesulfonate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 20h;
DOI:10.1002/1099-0690(200208)2002:16<2742::AID-EJOC2742>3.0.CO;2-R

Reference yield:

: 223131-81-5
4-tert-butyldimethylsilanyloxy-4-cyclohexyl-2-butanone

: 497069-73-5
3-tert-butyldimethylsilanyloxy-3-cyclohexyl-1-methylpropyl methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / NaBH₄ / ethanol / 20 h / 0 - 20 °C

2: 99 percent / NEt₃ / CH₂Cl₂ / 20 h / 0 - 20 °C

With sodium tetrahydroborate; triethylamine; In ethanol; dichloromethane;
DOI:10.1002/1099-0690(200208)2002:16<2742::AID-EJOC2742>3.0.CO;2-R

Reference yield:

: 2316-84-9
4-cyclohexyl-4-hydroxybutan-2-one

: 497069-73-5
3-tert-butyldimethylsilanyloxy-3-cyclohexyl-1-methylpropyl methanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / imidazole / dimethylformamide / 20 h / 0 - 20 °C

2: 100 percent / NaBH₄ / ethanol / 20 h / 0 - 20 °C

3: 99 percent / NEt₃ / CH₂Cl₂ / 20 h / 0 - 20 °C

With 1H-imidazole; sodium tetrahydroborate; triethylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/1099-0690(200208)2002:16<2742::AID-EJOC2742>3.0.CO;2-R