2-Butene, 1,1'-oxybis[3-methyl]

Base Information

• Chemical Name: 2-Butene, 1,1'-oxybis[3-methyl]
• CAS No.: 26902-25-0
• Molecular Formula: C10H18 O
• Molecular Weight: 154.252
• Hs Code.: 2909199090
• Mol file: 26902-25-0.mol

Synonyms:2-Butene,1,1'-oxybis[3-methyl- (9CI); Ether, bis(3-methyl-2-butenyl) (6CI,8CI);Bis(3-methyl-2-butenyl) ether; Diprenyl ether

Chemical Property of 2-Butene, 1,1'-oxybis[3-methyl]

Chemical Property:

• Boiling Point: 55 °C(Press: 3 Torr)
• PSA: 9.23000
• Density: 0.8380 g/cm3(Temp: 16 °C)
• LogP: 2.93540

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Butene, 1,1'-oxybis[3-methyl]

There total 17 articles about 2-Butene, 1,1'-oxybis[3-methyl] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

p-cresol (106-44-5) + 3-methyl-2-buten-1-ol (556-82-1) → 2,2,6-trimethyl-3,4-dihydro-2H-chromene (23446-57-3) + 3-methyl-1-(3-methylbut-2-enyloxy)but-2-ene (26902-25-0) + 4-methyl-2-(3-methyl-2-buten-1-yl)phenol (23446-56-2) + 1-methyl-4-(3-methylbut-2-enyloxy)benzene (23446-54-0)

Guidance literature:

With Zeolites ZSM; In n-heptane; at 100 ℃; for 10h;

DOI:10.1134/S1070363220030032

Reference yield: 47.0%

p-cresol (106-44-5) + 3-methyl-2-buten-1-ol (556-82-1) → 2,2,6-trimethyl-3,4-dihydro-2H-chromene (23446-57-3) + 3-methyl-1-(3-methylbut-2-enyloxy)but-2-ene (26902-25-0) + 4-methyl-2-(3-methyl-2-buten-1-yl)phenol (23446-56-2) + 1-methyl-4-(3-methylbut-2-enyloxy)benzene (23446-54-0) + 2,6-bis(2-methylbut-3-en-2-yl)-4-methylphenol + 2,6-bis(3-methylbut-2-en-1-yl)-4-methylphenol (82719-55-9)

Guidance literature:

With Zeolites ZSM; In n-heptane; at 100 ℃; for 5h;

DOI:10.1134/S1070363220030032

Reference yield: 42.0%

p-cresol (106-44-5) + 3-methyl-2-buten-1-ol (556-82-1) → 3-methyl-1-(3-methylbut-2-enyloxy)but-2-ene (26902-25-0) + 4-methyl-2-(3-methyl-2-buten-1-yl)phenol (23446-56-2) + 1-methyl-4-(3-methylbut-2-enyloxy)benzene (23446-54-0) + 2,6-bis(3-methylbut-2-en-1-yl)-4-methylphenol (82719-55-9) + 3,4-dihydro-2,2,6-trimethyl-8-(3-methyl-2-buten-1-yl)-2H-1-benzopyran (23446-59-5)

Guidance literature:

With aluminum isopropoxide; at 120 ℃; for 3.5h;

DOI:10.1134/S1070363220030032

upstream raw materials:

3-methyl-2-buten-1-ol

2-methyl-3-buten-2-ol

hydrogenchloride

Triethyl orthoacetate

Downstream raw materials:

2-methyl-1-buten-4-ol

(+/-)-lavandulol

(E/Z)-3,7-dimethyl-2,6-octadienal

i-Amyl alcohol