2-[4-(benzyloxy)-3-methoxyphenyl]-N-[3-(benzyloxy)-4-methoxyphenethyl]acetamide

Base Information

Chemical Name:2-[4-(benzyloxy)-3-methoxyphenyl]-N-[3-(benzyloxy)-4-methoxyphenethyl]acetamide
CAS No.:4672-96-2
Molecular Formula:C₃₂H₃₃NO₅
Molecular Weight:511.618
Hs Code.:

Synonyms:2-[4-(benzyloxy)-3-methoxyphenyl]-N-[3-(benzyloxy)-4-methoxyphenethyl]acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[4-(benzyloxy)-3-methoxyphenyl]-N-[3-(benzyloxy)-4-methoxyphenethyl]acetamide

Chemical Property:

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Technology Process of 2-[4-(benzyloxy)-3-methoxyphenyl]-N-[3-(benzyloxy)-4-methoxyphenethyl]acetamide

There total 12 articles about 2-[4-(benzyloxy)-3-methoxyphenyl]-N-[3-(benzyloxy)-4-methoxyphenethyl]acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 36455-21-7
3-benzyloxy-4-methoxyphenylethylamine

: 54313-35-8
2-(4-(benzyloxy)-3-methoxyphenyl)acetyl chloride

: 4672-96-2
2-[4-(benzyloxy)-3-methoxyphenyl]-N-[3-(benzyloxy)-4-methoxyphenethyl]acetamide

Guidance literature:: With sodium carbonate; In dichloromethane; water; at 20 ℃; for 3h;
DOI:10.1002/asia.201500611

Reference yield:

: 100-39-0
benzyl bromide

: 4672-96-2
2-[4-(benzyloxy)-3-methoxyphenyl]-N-[3-(benzyloxy)-4-methoxyphenethyl]acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / ethanol / 3 h / Reflux

2: ammonium acetate; acetic acid / 0.5 h / Reflux

3: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

4: sodium carbonate / dichloromethane; water / 3 h / 20 °C

With lithium aluminium tetrahydride; ammonium acetate; sodium carbonate; potassium carbonate; acetic acid; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1002/asia.201500611

Reference yield:

: 621-59-0
isovanillin

: 4672-96-2
2-[4-(benzyloxy)-3-methoxyphenyl]-N-[3-(benzyloxy)-4-methoxyphenethyl]acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / ethanol / 3 h / Reflux

2: ammonium acetate; acetic acid / 0.5 h / Reflux

3: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

4: sodium carbonate / dichloromethane; water / 3 h / 20 °C

With lithium aluminium tetrahydride; ammonium acetate; sodium carbonate; potassium carbonate; acetic acid; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1002/asia.201500611