4-chloro-2-(3-chlorophenylcarbamoyl)phenyl nonylcarbamate

Base Information

• Chemical Name: 4-chloro-2-(3-chlorophenylcarbamoyl)phenyl nonylcarbamate
• CAS No.: 1219818-66-2
• Molecular Formula: C₂₃H₂₈Cl₂N₂O₃
• Molecular Weight: 451.393
• Mol file: 1219818-66-2.mol

Synonyms:4-chloro-2-(3-chlorophenylcarbamoyl)phenyl nonylcarbamate

Chemical Property of 4-chloro-2-(3-chlorophenylcarbamoyl)phenyl nonylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-chloro-2-(3-chlorophenylcarbamoyl)phenyl nonylcarbamate

There total 3 articles about 4-chloro-2-(3-chlorophenylcarbamoyl)phenyl nonylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

nonyl isocyanate (4184-73-0) + 3',5-dichlorosalicylanilide (22203-98-1) → 4-chloro-2-(3-chlorophenylcarbamoyl)phenyl nonylcarbamate (1219818-66-2)

Guidance literature:

3',5-dichlorosalicylanilide; With triethylamine; In acetonitrile;

nonyl isocyanate; In acetonitrile; at 20 ℃;

DOI:10.1016/j.bmc.2009.12.055

Reference yield:

3-chloro-aniline (108-42-9) → 4-chloro-2-(3-chlorophenylcarbamoyl)phenyl nonylcarbamate (1219818-66-2)

Guidance literature:

Multi-step reaction with 2 steps

1: phosphorus trichloride / chlorobenzene / Microwave irradiation

2: triethylamine / acetonitrile / 20 °C

With triethylamine; phosphorus trichloride; In chlorobenzene; acetonitrile;

DOI:10.1016/j.bmcl.2011.05.118

Reference yield:

5-chloro-2-hydroxybenzoic acid (321-14-2) → 4-chloro-2-(3-chlorophenylcarbamoyl)phenyl nonylcarbamate (1219818-66-2)

Guidance literature:

Multi-step reaction with 2 steps

1: phosphorus trichloride / chlorobenzene / Microwave irradiation

2: triethylamine / acetonitrile / 20 °C

With triethylamine; phosphorus trichloride; In chlorobenzene; acetonitrile;

DOI:10.1016/j.bmcl.2011.05.118

upstream raw materials:

nonyl isocyanate

3',5-dichlorosalicylanilide

5-chloro-2-hydroxybenzoic acid

3-chloro-aniline