C₄₆H₇₄O₄S₂Si

Base Information

Chemical Name:C₄₆H₇₄O₄S₂Si
CAS No.:259177-52-1
Molecular Formula:C₄₆H₇₄O₄S₂Si
Molecular Weight:783.309
Hs Code.:

C<sub>46</sub>H<sub>74</sub>O<sub>4</sub>S<sub>2</sub>Si

Synonyms:C₄₆H₇₄O₄S₂Si

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Chemical Property of C₄₆H₇₄O₄S₂Si

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Technology Process of C₄₆H₇₄O₄S₂Si

There total 11 articles about C₄₆H₇₄O₄S₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52646-93-2
[(S)-2,6,6-trimethylcyclohex-2-enyl]methanol

: 259177-52-1
C₄₆H₇₄O₄S₂Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: PPh₃,; I₂,; imidazole / benzene

2.1: tert-butyllithium

2.2: -78 °C

3.1: n-BuLi

With 1H-imidazole; n-butyllithium; iodine; tert.-butyl lithium; triphenylphosphine; In benzene; 1.1: Iodination / 2.1: Metallation / 2.2: Addition / 3.1: Metallation / 3.2: Addition / 3.3: Methylation;
DOI:10.1021/ja9934091

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 259177-52-1
C₄₆H₇₄O₄S₂Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: lutidine

2.1: Pd(PPh₃)4,; pyrrolidine

3.1: Cs₂CO₃

4.1: Pd(dppp),; (n-Bu)3N,; HCO₂H

5.1: H₂ / Pd/C

6.1: 'Dess-Martin reagent

7.1: tert-butyllithium

7.2: -78 °C

8.1: n-BuLi

With pyrrolidine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; formic acid; tributyl-amine; lutidine; Pd(dppp); hydrogen; tert.-butyl lithium; caesium carbonate; Dess-Martin periodane; palladium on activated charcoal; 1.1: silylation / 2.1: deallylation / 3.1: triflation / 4.1: Reduction / 5.1: Hydrogenolysis / 6.1: Oxidation / 7.1: Metallation / 7.2: Addition / 8.1: Metallation / 8.2: Addition / 8.3: Methylation;
DOI:10.1021/ja9934091

Reference yield:

: 259177-47-4
(1R,2S,4aR,4bS,6aS,11aS,11bR,13aR)-9-Allyloxy-1-benzyloxymethyl-7,10-dimethoxy-1,4a,6a,11b-tetramethyl-2,3,4,4a,4b,5,6,6a,11,11a,11b,12,13,13a-tetradecahydro-1H-indeno[2,1-a]phenanthren-2-ol

: 259177-52-1
C₄₆H₇₄O₄S₂Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: lutidine

2.1: Pd(PPh₃)4,; pyrrolidine

3.1: Cs₂CO₃

4.1: Pd(dppp),; (n-Bu)3N,; HCO₂H

5.1: H₂ / Pd/C

6.1: 'Dess-Martin reagent

7.1: tert-butyllithium

7.2: -78 °C

8.1: n-BuLi

With pyrrolidine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; formic acid; tributyl-amine; lutidine; Pd(dppp); hydrogen; tert.-butyl lithium; caesium carbonate; Dess-Martin periodane; palladium on activated charcoal; 1.1: silylation / 2.1: deallylation / 3.1: triflation / 4.1: Reduction / 5.1: Hydrogenolysis / 6.1: Oxidation / 7.1: Metallation / 7.2: Addition / 8.1: Metallation / 8.2: Addition / 8.3: Methylation;
DOI:10.1021/ja9934091