benzyl-3,4-di-(2-benzyloxycarbonylmethyl)-5-methyl-2-pyrrole carboxylate

Base Information

Chemical Name:benzyl-3,4-di-(2-benzyloxycarbonylmethyl)-5-methyl-2-pyrrole carboxylate
CAS No.:162661-74-7
Molecular Formula:C₃₁H₂₉NO₆
Molecular Weight:511.574
Hs Code.:

Synonyms:benzyl-3,4-di-(2-benzyloxycarbonylmethyl)-5-methyl-2-pyrrole carboxylate

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Chemical Property of benzyl-3,4-di-(2-benzyloxycarbonylmethyl)-5-methyl-2-pyrrole carboxylate

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Technology Process of benzyl-3,4-di-(2-benzyloxycarbonylmethyl)-5-methyl-2-pyrrole carboxylate

There total 5 articles about benzyl-3,4-di-(2-benzyloxycarbonylmethyl)-5-methyl-2-pyrrole carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 73869-96-2
Methyl-5-methoxycarbonyl-4-methoxycarbonylmethyl-2-methylpyrrol-3-acetat

: 100-51-6,185532-71-2
benzyl alcohol

: 162661-74-7
benzyl-3,4-di-(2-benzyloxycarbonylmethyl)-5-methyl-2-pyrrole carboxylate

Guidance literature:: Methyl-5-methoxycarbonyl-4-methoxycarbonylmethyl-2-methylpyrrol-3-acetat; benzyl alcohol; at 220 ℃; Inert atmosphere;

With sodium; at 220 ℃;
DOI:10.1039/c6nj00517a

Reference yield: 66.0%

: 100-44-7
benzyl chloride

: 162661-73-6
3,4-Bis-carboxymethyl-5-methyl-1H-pyrrole-2-carboxylic acid

: 162661-74-7
benzyl-3,4-di-(2-benzyloxycarbonylmethyl)-5-methyl-2-pyrrole carboxylate

Guidance literature:: In triethylamine; N,N-dimethyl-formamide; at 20 ℃; for 72h;
DOI:10.1016/0040-4020(94)01103-7

Reference yield:

: 101116-14-7
(4-acetyl-2-ethoxycarbonyl-5-methyl-pyrrol-3-yl)-acetic acid ethyl ester

: 162661-74-7
benzyl-3,4-di-(2-benzyloxycarbonylmethyl)-5-methyl-2-pyrrole carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / 70percent perchloric acid, thallium(III) nitrate / 5 h / 20 °C

2: 68 percent / 1.) 1N NaOH, 2.) hydrochloric acid / ethanol; H₂O

3: 66 percent / dimethylformamide; triethylamine / 72 h / 20 °C

With hydrogenchloride; sodium hydroxide; perchloric acid; thallium(III) nitrate; In ethanol; water; triethylamine; N,N-dimethyl-formamide;
DOI:10.1016/0040-4020(94)01103-7