Methyl-5-benzyloxycarbonyl-4-methoxycarbonylmethyl-2-methylpyrrol-3-acetat

Base Information

• Chemical Name: Methyl-5-benzyloxycarbonyl-4-methoxycarbonylmethyl-2-methylpyrrol-3-acetat
• CAS No.: 73869-98-4
• Molecular Formula: C₁₉H₂₁NO₆
• Molecular Weight: 359.379

Synonyms:Methyl-5-benzyloxycarbonyl-4-methoxycarbonylmethyl-2-methylpyrrol-3-acetat

Chemical Property of Methyl-5-benzyloxycarbonyl-4-methoxycarbonylmethyl-2-methylpyrrol-3-acetat

Chemical Property:

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Technology Process of Methyl-5-benzyloxycarbonyl-4-methoxycarbonylmethyl-2-methylpyrrol-3-acetat

There total 15 articles about Methyl-5-benzyloxycarbonyl-4-methoxycarbonylmethyl-2-methylpyrrol-3-acetat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

methanol (67-56-1) + sodium methylate (124-41-4) + benzyl-3,4-di-(2-benzyloxycarbonylmethyl)-5-methyl-2-pyrrole carboxylate (162661-74-7) → Methyl-5-benzyloxycarbonyl-4-methoxycarbonylmethyl-2-methylpyrrol-3-acetat (73869-98-4)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 3h;

DOI:10.1039/c6nj00517a

Reference yield: 62.0%

methanol (67-56-1) + 5-Benzyloxycarbonyl-4-carboxymethyl-2-methylpyrrol-3-essigsaeure (73869-97-3) → Methyl-5-benzyloxycarbonyl-4-methoxycarbonylmethyl-2-methylpyrrol-3-acetat (73869-98-4)

Guidance literature:

With hydrogenchloride; at 25 ℃; for 24h;

Reference yield:

Methyl-5-methoxycarbonyl-4-methoxycarbonylmethyl-2-methylpyrrol-3-acetat (73869-96-2) + benzyl alcohol (100-51-6,185532-71-2) → Methyl-5-benzyloxycarbonyl-4-methoxycarbonylmethyl-2-methylpyrrol-3-acetat (73869-98-4)

Guidance literature:

With sodium; at 100 - 110 ℃; for 3h; under 30 Torr;

upstream raw materials:

methanol

5-Benzyloxycarbonyl-4-carboxymethyl-2-methylpyrrol-3-essigsaeure

benzyl 4-acetyl-3-methoxycarbonylmethyl-5-methylpyrrole-2-carboxylate

Methyl-5-methoxycarbonyl-4-methoxycarbonylmethyl-2-methylpyrrol-3-acetat

Downstream raw materials:

Methyl-2-acetoxymethyl-5-benzylcarbonyl-4-methoxycarbonylmethylpyrrol-3-acetat

Methyl-5-benzyloxycarbonyl-2-formyl-4-methoxycarbonylmethylpyrrol-3-acetat

dibenzyl 3,3',4,4'-tetramethoxycarbonylmethyl-2,2'-methylenedipyrrole-5,5'-dicarboxylate

benzyl 3,4-di(2-acetoxyethyl)-5-acetoxymethylpyrrole-2-carboxylate

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