3,4-diphenylthiophene-2,5-diylbis(methylene-N,N-diethyldithiocarbamate)

Base Information

Chemical Name:3,4-diphenylthiophene-2,5-diylbis(methylene-N,N-diethyldithiocarbamate)
CAS No.:836606-04-3
Molecular Formula:C₂₈H₃₄N₂S₅
Molecular Weight:558.921
Hs Code.:

Synonyms:3,4-diphenylthiophene-2,5-diylbis(methylene-N,N-diethyldithiocarbamate)

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Chemical Property of 3,4-diphenylthiophene-2,5-diylbis(methylene-N,N-diethyldithiocarbamate)

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Technology Process of 3,4-diphenylthiophene-2,5-diylbis(methylene-N,N-diethyldithiocarbamate)

There total 8 articles about 3,4-diphenylthiophene-2,5-diylbis(methylene-N,N-diethyldithiocarbamate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 181218-41-7
3,4-diphenyl-2,5-bis(chloromethyl)thiophene

: 148-18-5
sodium N,N-diethyldithiocarbamate

: 836606-04-3
3,4-diphenylthiophene-2,5-diylbis(methylene-N,N-diethyldithiocarbamate)

Guidance literature:: In methanol; at 20 ℃; for 3h;
DOI:10.1021/ma047940e

Reference yield:

: 98-80-6
phenylboronic acid

: 836606-04-3
3,4-diphenylthiophene-2,5-diylbis(methylene-N,N-diethyldithiocarbamate)

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / KF / Pd(PPh₃)4 / H₂O; toluene / 18 h / Heating

2: 98 percent / HCl; Ac₂O / 4.5 h / 70 °C

3: 70 percent / methanol / 3 h / 20 °C

With hydrogenchloride; potassium fluoride; acetic anhydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; water; toluene;
DOI:10.1021/ma047940e

Reference yield:

: 2461-80-5
diphenacyl sulfide

: 836606-04-3
3,4-diphenylthiophene-2,5-diylbis(methylene-N,N-diethyldithiocarbamate)

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / Zn; TiCl₄ / tetrahydrofuran / 3 h / 0 - 15 °C

2: 77 percent / TsOH*H₂O / benzene / 4 h / Heating

3: 98 percent / HCl; Ac₂O / 4.5 h / 70 °C

4: 70 percent / methanol / 3 h / 20 °C

With hydrogenchloride; acetic anhydride; titanium tetrachloride; toluene-4-sulfonic acid; zinc; In tetrahydrofuran; methanol; benzene;
DOI:10.1021/ma047940e