2,2-Dimethyl-propionic acid 1-benzyl-2,6-dioxo-1,2,6,7-tetrahydro-purin-3-ylmethyl ester

Base Information

Chemical Name:2,2-Dimethyl-propionic acid 1-benzyl-2,6-dioxo-1,2,6,7-tetrahydro-purin-3-ylmethyl ester
CAS No.:205928-51-4
Molecular Formula:C₁₈H₂₀N₄O₄
Molecular Weight:356.381
Hs Code.:

Synonyms:2,2-Dimethyl-propionic acid 1-benzyl-2,6-dioxo-1,2,6,7-tetrahydro-purin-3-ylmethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2-Dimethyl-propionic acid 1-benzyl-2,6-dioxo-1,2,6,7-tetrahydro-purin-3-ylmethyl ester

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Technology Process of 2,2-Dimethyl-propionic acid 1-benzyl-2,6-dioxo-1,2,6,7-tetrahydro-purin-3-ylmethyl ester

There total 4 articles about 2,2-Dimethyl-propionic acid 1-benzyl-2,6-dioxo-1,2,6,7-tetrahydro-purin-3-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 205928-48-9
2,2-Dimethyl-propionic acid 1,7-dibenzyl-2,6-dioxo-1,2,6,7-tetrahydro-purin-3-ylmethyl ester

: 205928-51-4
2,2-Dimethyl-propionic acid 1-benzyl-2,6-dioxo-1,2,6,7-tetrahydro-purin-3-ylmethyl ester

Guidance literature:: With hydrogen; acetic acid; palladium dihydroxide; for 20h; under 2482.3 Torr;
DOI:10.1080/07328319808004673

Reference yield:

: 18997-19-8
Chloromethyl pivalate

: 205928-51-4
2,2-Dimethyl-propionic acid 1-benzyl-2,6-dioxo-1,2,6,7-tetrahydro-purin-3-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium hydride / 1.) DMF, 15 min; other reagent: potassium carbonate, 2.) DMF, room temperature, 4 h

2: 76 percent / potassium carbonate / dimethylformamide / 5 h / 50 °C

3: 86 percent / acetic acid, hydrogen / palladium hydroxide on carbon / 20 h / 2482.3 Torr

With hydrogen; sodium hydride; potassium carbonate; acetic acid; palladium dihydroxide; In N,N-dimethyl-formamide;
DOI:10.1080/07328319808004673

Reference yield:

: 56160-64-6
7-benzylxanthine

: 205928-51-4
2,2-Dimethyl-propionic acid 1-benzyl-2,6-dioxo-1,2,6,7-tetrahydro-purin-3-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium hydride / 1.) DMF, 15 min; other reagent: potassium carbonate, 2.) DMF, room temperature, 4 h

2: 76 percent / potassium carbonate / dimethylformamide / 5 h / 50 °C

3: 86 percent / acetic acid, hydrogen / palladium hydroxide on carbon / 20 h / 2482.3 Torr

With hydrogen; sodium hydride; potassium carbonate; acetic acid; palladium dihydroxide; In N,N-dimethyl-formamide;
DOI:10.1080/07328319808004673