2,2-Dimethyl-propionic acid 1,7-dibenzyl-2,6-dioxo-1,2,6,7-tetrahydro-purin-3-ylmethyl ester

Base Information

Chemical Name:2,2-Dimethyl-propionic acid 1,7-dibenzyl-2,6-dioxo-1,2,6,7-tetrahydro-purin-3-ylmethyl ester
CAS No.:205928-48-9
Molecular Formula:C₂₅H₂₆N₄O₄
Molecular Weight:446.506
Hs Code.:

Synonyms:2,2-Dimethyl-propionic acid 1,7-dibenzyl-2,6-dioxo-1,2,6,7-tetrahydro-purin-3-ylmethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2-Dimethyl-propionic acid 1,7-dibenzyl-2,6-dioxo-1,2,6,7-tetrahydro-purin-3-ylmethyl ester

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Technology Process of 2,2-Dimethyl-propionic acid 1,7-dibenzyl-2,6-dioxo-1,2,6,7-tetrahydro-purin-3-ylmethyl ester

There total 3 articles about 2,2-Dimethyl-propionic acid 1,7-dibenzyl-2,6-dioxo-1,2,6,7-tetrahydro-purin-3-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 100-39-0
benzyl bromide

: 205928-47-8
2,2-Dimethylpropionic acid [7-benzyl-2,6-dioxo-1,2,6,7-tetrahydropurin-3-yl]methyl ester

: 205928-48-9
2,2-Dimethyl-propionic acid 1,7-dibenzyl-2,6-dioxo-1,2,6,7-tetrahydro-purin-3-ylmethyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 5h;
DOI:10.1080/07328319808004673

Reference yield:

: 18997-19-8
Chloromethyl pivalate

: 205928-48-9
2,2-Dimethyl-propionic acid 1,7-dibenzyl-2,6-dioxo-1,2,6,7-tetrahydro-purin-3-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium hydride / 1.) DMF, 15 min; other reagent: potassium carbonate, 2.) DMF, room temperature, 4 h

2: 76 percent / potassium carbonate / dimethylformamide / 5 h / 50 °C

With sodium hydride; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1080/07328319808004673

Reference yield:

: 56160-64-6
7-benzylxanthine

: 205928-48-9
2,2-Dimethyl-propionic acid 1,7-dibenzyl-2,6-dioxo-1,2,6,7-tetrahydro-purin-3-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium hydride / 1.) DMF, 15 min; other reagent: potassium carbonate, 2.) DMF, room temperature, 4 h

2: 76 percent / potassium carbonate / dimethylformamide / 5 h / 50 °C

With sodium hydride; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1080/07328319808004673