6-(7-(2-(4-chlorophenylamino)benzo[d]oxazol-5-yloxy)thieno[3,2-b]pyridin-2-yl)nicotinaldehyde

Base Information

Chemical Name:6-(7-(2-(4-chlorophenylamino)benzo[d]oxazol-5-yloxy)thieno[3,2-b]pyridin-2-yl)nicotinaldehyde
CAS No.:1430331-42-2
Molecular Formula:C₂₆H₁₅ClN₄O₃S
Molecular Weight:498.949
Hs Code.:

Synonyms:6-(7-(2-(4-chlorophenylamino)benzo[d]oxazol-5-yloxy)thieno[3,2-b]pyridin-2-yl)nicotinaldehyde

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Chemical Property of 6-(7-(2-(4-chlorophenylamino)benzo[d]oxazol-5-yloxy)thieno[3,2-b]pyridin-2-yl)nicotinaldehyde

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Technology Process of 6-(7-(2-(4-chlorophenylamino)benzo[d]oxazol-5-yloxy)thieno[3,2-b]pyridin-2-yl)nicotinaldehyde

There total 6 articles about 6-(7-(2-(4-chlorophenylamino)benzo[d]oxazol-5-yloxy)thieno[3,2-b]pyridin-2-yl)nicotinaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1430331-41-1
5-(2-(5-(1,3-dioxolan-2-yl)pyridin-2-yl)thieno[3,2-b]pyridin-7-yloxy)-N-(4-chlorophenyl)benzo[d]oxazol-2-amine

: 1430331-42-2
6-(7-(2-(4-chlorophenylamino)benzo[d]oxazol-5-yloxy)thieno[3,2-b]pyridin-2-yl)nicotinaldehyde

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water; at 20 - 50 ℃; for 3h;

Reference yield:

: 1430331-37-5
2-(4-chlorophenylamino)benzo[d]oxazol-5-yl benzoate

: 1430331-42-2
6-(7-(2-(4-chlorophenylamino)benzo[d]oxazol-5-yloxy)thieno[3,2-b]pyridin-2-yl)nicotinaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: methanol; potassium carbonate / tetrahydrofuran / 2 h / 20 °C

2: potassium tert-butylate / dimethyl sulfoxide / 1 h / 20 - 90 °C

3: hydrogenchloride / tetrahydrofuran; water / 3 h / 20 - 50 °C

With hydrogenchloride; methanol; potassium tert-butylate; potassium carbonate; In tetrahydrofuran; water; dimethyl sulfoxide;

Reference yield:

: 1430331-35-3
3-(3-(4-Chlorophenyl)thioureido)-4-hydroxyphenyl benzoate

: 1430331-42-2
6-(7-(2-(4-chlorophenylamino)benzo[d]oxazol-5-yloxy)thieno[3,2-b]pyridin-2-yl)nicotinaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / Reflux

2: methanol; potassium carbonate / tetrahydrofuran / 2 h / 20 °C

3: potassium tert-butylate / dimethyl sulfoxide / 1 h / 20 - 90 °C

4: hydrogenchloride / tetrahydrofuran; water / 3 h / 20 - 50 °C

With hydrogenchloride; methanol; potassium tert-butylate; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; water; dimethyl sulfoxide;