4-bromo-3-chloro-N-trimethylsilanylmethyl-thiobenzimidic acid methyl ester

Base Information

Chemical Name:4-bromo-3-chloro-N-trimethylsilanylmethyl-thiobenzimidic acid methyl ester
CAS No.:1370257-48-9
Molecular Formula:C₁₂H₁₇BrClNSSi
Molecular Weight:350.782
Hs Code.:

Synonyms:4-bromo-3-chloro-N-trimethylsilanylmethyl-thiobenzimidic acid methyl ester

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Chemical Property of 4-bromo-3-chloro-N-trimethylsilanylmethyl-thiobenzimidic acid methyl ester

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Technology Process of 4-bromo-3-chloro-N-trimethylsilanylmethyl-thiobenzimidic acid methyl ester

There total 3 articles about 4-bromo-3-chloro-N-trimethylsilanylmethyl-thiobenzimidic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1370257-47-8
4-bromo-3-chloro-N-trimethylsilanylmethyl-thiobenzamide

: 74-88-4
methyl iodide

: 1370257-48-9
4-bromo-3-chloro-N-trimethylsilanylmethyl-thiobenzimidic acid methyl ester

Guidance literature:: With caesium carbonate; In tetrahydrofuran; at -5 - 40 ℃;

Reference yield:

: 25118-59-6
4-bromo-3-chlorobenzoic acid

: 1370257-48-9
4-bromo-3-chloro-N-trimethylsilanylmethyl-thiobenzimidic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / 20 °C

1.2: 20 °C

2.1: Lawessons reagent / toluene / 1 h / Reflux

3.1: caesium carbonate / tetrahydrofuran / -5 - 40 °C

With Lawessons reagent; dmap; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane; toluene;

Reference yield:

: 1370257-46-7
4-bromo-3-chloro-N-trimethylsilanylmethyl-benzamide

: 1370257-48-9
4-bromo-3-chloro-N-trimethylsilanylmethyl-thiobenzimidic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Lawessons reagent / toluene / 1 h / Reflux

2: caesium carbonate / tetrahydrofuran / -5 - 40 °C

With Lawessons reagent; caesium carbonate; In tetrahydrofuran; toluene;