phenyl (E)-β-(trifluoromethyl)vinyl sulfide

Base Information

Chemical Name:phenyl (E)-β-(trifluoromethyl)vinyl sulfide
CAS No.:102687-66-1
Molecular Formula:C₉H₇F₃S
Molecular Weight:204.216
Hs Code.:

Synonyms:phenyl (E)-β-(trifluoromethyl)vinyl sulfide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl (E)-β-(trifluoromethyl)vinyl sulfide

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Technology Process of phenyl (E)-β-(trifluoromethyl)vinyl sulfide

There total 5 articles about phenyl (E)-β-(trifluoromethyl)vinyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1514-82-5
2-bromo-3,3,3-trifluoropropene

: 108-98-5
thiophenol

: 102687-66-1
phenyl (E)-β-(trifluoromethyl)vinyl sulfide

Guidance literature:: With potassium hydroxide; In ethanol; at 0 - 20 ℃;
DOI:10.1039/c8ob00293b

Reference yield: 23.0%

: 754-12-1
2,3,3,3-tetrafluoro-propene

: 108-98-5
thiophenol

: 102687-66-1
phenyl (E)-β-(trifluoromethyl)vinyl sulfide

Guidance literature:: thiophenol; With sodium hydride; In hexane; N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 0.5h; Inert atmosphere;

2,3,3,3-tetrafluoro-propene; In hexane; N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1002/ejoc.201901445