2-chlorophenyl fluorosulfate

Base Information

• Chemical Name: 2-chlorophenyl fluorosulfate
• CAS No.: 16475-32-4
• Molecular Formula: C₆H₄ClFO₃S
• Molecular Weight: 210.613
• Mol file: 16475-32-4.mol

Synonyms:2-chlorophenyl fluorosulfate

Chemical Property of 2-chlorophenyl fluorosulfate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 2-chlorophenyl fluorosulfate

There total 2 articles about 2-chlorophenyl fluorosulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-monochlorophenol (95-57-8) → 2-chlorophenyl fluorosulfate (16475-32-4)

Guidance literature:

With fluorosulfonyl fluoride; triethylamine; In dimethyl sulfoxide; at 20 ℃; for 2h;

DOI:10.1002/asia.201700891

Reference yield:

→ 2-chlorophenyl fluorosulfate (16475-32-4)

Guidance literature:

Aus Trimethyl(o-chlorophenoxy)silan und Thionyltetrafluorid;

Reference yield: 83.0%

2-chlorophenyl fluorosulfate (16475-32-4) + 1H-2-amino-4-toluoylpyrazole (90861-52-2) → o-chlorophenyl-5-methyl-3-p-tolyl-1-hydropyrazol-1-sulfonate

Guidance literature:

With potassium tert-butylate; In dimethyl sulfoxide; at 70 ℃; for 10h; Inert atmosphere;

DOI:10.1016/j.bmc.2021.116344

upstream raw materials:

2-monochlorophenol

Downstream raw materials:

ethyl 2-chlorobenzoate

ortho-chlorobenzoic acid