trans-4-(3-hydroxyphenyl)-4-methylpipecolylglycylglycylphenylalanylleucinamide hydrochloride

Base Information

Chemical Name:trans-4-(3-hydroxyphenyl)-4-methylpipecolylglycylglycylphenylalanylleucinamide hydrochloride
CAS No.:103320-90-7
Molecular Formula:C₃₂H₄₄N₆O₆*ClH
Molecular Weight:645.199
Hs Code.:

Synonyms:trans-4-(3-hydroxyphenyl)-4-methylpipecolylglycylglycylphenylalanylleucinamide hydrochloride

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Chemical Property of trans-4-(3-hydroxyphenyl)-4-methylpipecolylglycylglycylphenylalanylleucinamide hydrochloride

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Technology Process of trans-4-(3-hydroxyphenyl)-4-methylpipecolylglycylglycylphenylalanylleucinamide hydrochloride

There total 6 articles about trans-4-(3-hydroxyphenyl)-4-methylpipecolylglycylglycylphenylalanylleucinamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 103305-05-1
cis-N-benzyl-4-(3-hydroxyphenyl)-4-methylpipecolylglycylglycylphenylalanylleucinamide hydrochloride

: 103320-90-7
cis-4-(3-hydroxyphenyl)-4-methylpipecolylglycylglycylphenylalanylleucinamide hydrochloride

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; Ambient temperature;
DOI:10.1021/jm00160a039

Reference yield: 72.0%

: 103305-05-1
trans-N-benzyl-4-(3-hydroxyphenyl)-4-methylpipecolylglycylglycylphenylalanylleucinamide hydrochloride

: 103320-90-7
trans-4-(3-hydroxyphenyl)-4-methylpipecolylglycylglycylphenylalanylleucinamide hydrochloride

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; Ambient temperature;
DOI:10.1021/jm00160a039

Reference yield:

: 81638-87-1
hydrochloride of amide of glycylglycyl-L-phenylalanyl-L-leucine

: 103320-90-7
cis-4-(3-hydroxyphenyl)-4-methylpipecolylglycylglycylphenylalanylleucinamide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / hydroxybenzotriazole, triethylamine, dicyclohexylcarbodiimide / dimethylformamide / 48 h

2: 76 percent / hydrogen / 10percent Pd/C / methanol / Ambient temperature

With hydrogen; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00160a039