hydrochloride of amide of glycylglycyl-L-phenylalanyl-L-leucine

Base Information

Chemical Name:hydrochloride of amide of glycylglycyl-L-phenylalanyl-L-leucine
CAS No.:81638-87-1
Molecular Formula:C₁₉H₂₉N₅O₄*ClH
Molecular Weight:427.931
Hs Code.:

Synonyms:hydrochloride of amide of glycylglycyl-L-phenylalanyl-L-leucine

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Chemical Property of hydrochloride of amide of glycylglycyl-L-phenylalanyl-L-leucine

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Technology Process of hydrochloride of amide of glycylglycyl-L-phenylalanyl-L-leucine

There total 9 articles about hydrochloride of amide of glycylglycyl-L-phenylalanyl-L-leucine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81638-86-0
(S)-2-((S)-2-amino-3-phenylpropanamido)-4-methylpentanamide hydrochloride

: 81638-87-1
hydrochloride of amide of glycylglycyl-L-phenylalanyl-L-leucine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NH₃, 2.) AcOH / 1.) THF, CHCl₃, 2.) THF, 24 h

2: 98 percent / 2 M HCl / acetic acid / 0.75 h

With hydrogenchloride; ammonia; acetic acid; In acetic acid;

Reference yield:

: 74257-73-1
tert-butyl ((S)-1-(((S)-1-amino-4-methyl-1-oxopentan-2-yl)amino)-1-oxo-3-phenylpropan-2-yl)carbamate

: 81638-87-1
hydrochloride of amide of glycylglycyl-L-phenylalanyl-L-leucine

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / 2 M HCl / acetic acid / 0.75 h

2: 1.) NH₃, 2.) AcOH / 1.) THF, CHCl₃, 2.) THF, 24 h

3: 98 percent / 2 M HCl / acetic acid / 0.75 h

With hydrogenchloride; ammonia; acetic acid; In acetic acid;

Reference yield:

: 93200-07-8,93200-08-9
Boc-Gly-Phe-Leu-NH₂

: 81638-87-1
hydrochloride of amide of glycylglycyl-L-phenylalanyl-L-leucine

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid / 1 h / 20 °C

2: 4-methyl-morpholine; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride / water / 12 h / 20 °C

3: trifluoroacetic acid / 1 h / 20 °C

With 4-methyl-morpholine; trifluoroacetic acid; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; In water;
DOI:10.1002/psc.1367