2-(N-(tert-butoxycarbonylmethyl)-N-{N'-[m-(2-propenyloxycarbonyl)phenyl]ureidomethylcarbonyl}amino)benzophenone

Base Information

Chemical Name:2-(N-(tert-butoxycarbonylmethyl)-N-{N'-[m-(2-propenyloxycarbonyl)phenyl]ureidomethylcarbonyl}amino)benzophenone
CAS No.:171724-14-4
Molecular Formula:C₃₂H₃₃N₃O₇
Molecular Weight:571.63
Hs Code.:

Synonyms:2-(N-(tert-butoxycarbonylmethyl)-N-{N'-[m-(2-propenyloxycarbonyl)phenyl]ureidomethylcarbonyl}amino)benzophenone

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Chemical Property of 2-(N-(tert-butoxycarbonylmethyl)-N-{N'-[m-(2-propenyloxycarbonyl)phenyl]ureidomethylcarbonyl}amino)benzophenone

Chemical Property:

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Technology Process of 2-(N-(tert-butoxycarbonylmethyl)-N-{N'-[m-(2-propenyloxycarbonyl)phenyl]ureidomethylcarbonyl}amino)benzophenone

There total 4 articles about 2-(N-(tert-butoxycarbonylmethyl)-N-{N'-[m-(2-propenyloxycarbonyl)phenyl]ureidomethylcarbonyl}amino)benzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29176-45-2
2-(N-Cbz-glycylamino)benzophenone

: 171724-14-4
2-(N-(tert-butoxycarbonylmethyl)-N-{N'-[m-(2-propenyloxycarbonyl)phenyl]ureidomethylcarbonyl}amino)benzophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / 30percent aq. HBr, AcOH / 1 h

2: Et₃N / dimethylformamide / 1.) 0 deg C, 30 min, 2.) RT, overnight

3: K₂CO₃, KI / dimethylformamide

With hydrogen bromide; potassium carbonate; acetic acid; triethylamine; potassium iodide; In N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(97)00104-1

Reference yield:

: 2835-77-0
(2-aminophenyl)(phenyl)methanone

: 171724-14-4
2-(N-(tert-butoxycarbonylmethyl)-N-{N'-[m-(2-propenyloxycarbonyl)phenyl]ureidomethylcarbonyl}amino)benzophenone

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) SOCl₂, HMPA / 1.) CH₃CN, -5 deg C, 10 min, 2.) CH₃CN, RT, 3 h

2: 92 percent / 30percent aq. HBr, AcOH / 1 h

3: Et₃N / dimethylformamide / 1.) 0 deg C, 30 min, 2.) RT, overnight

4: K₂CO₃, KI / dimethylformamide

With N,N,N,N,N,N-hexamethylphosphoric triamide; thionyl chloride; hydrogen bromide; potassium carbonate; acetic acid; triethylamine; potassium iodide; In N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(97)00104-1

Reference yield:

: 2-(glycylamino)benzophenone hydrobromide

: 171724-14-4
2-(N-(tert-butoxycarbonylmethyl)-N-{N'-[m-(2-propenyloxycarbonyl)phenyl]ureidomethylcarbonyl}amino)benzophenone

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / dimethylformamide / 1.) 0 deg C, 30 min, 2.) RT, overnight

2: K₂CO₃, KI / dimethylformamide

With potassium carbonate; triethylamine; potassium iodide; In N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(97)00104-1