C₂₈H₃₁N₃O₅

Base Information

Chemical Name:C₂₈H₃₁N₃O₅
CAS No.:1362022-57-8
Molecular Formula:C₂₈H₃₁N₃O₅
Molecular Weight:489.571
Hs Code.:

C<sub>28</sub>H<sub>31</sub>N<sub>3</sub>O<sub>5</sub>

Synonyms:C₂₈H₃₁N₃O₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₈H₃₁N₃O₅

Chemical Property:

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Technology Process of C₂₈H₃₁N₃O₅

There total 6 articles about C₂₈H₃₁N₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1362022-50-1
C₂₇H₂₉N₃O₅

: 74-88-4
methyl iodide

: 1362022-57-8
C₂₈H₃₁N₃O₅

Guidance literature:: C₂₇H₂₉N₃O₅; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

methyl iodide; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1039/c2cc17393j

Reference yield:

: 1235999-57-1
(2R,4aR,7R,8R,8aS)-6-(benzyloxy)-2-phenylhexahydropyrano[3,2-d][1,3]dioxine-7,8-diol

: 1362022-57-8
C₂₈H₃₁N₃O₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine / dichloromethane / 3 h / -20 - 0 °C

2.1: tetrabutylammoniun azide / toluene / 2.5 h / 65 - 100 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

3.2: 0 - 20 °C

4.1: triethylsilane; phenylborondichloride / dichloromethane / 1.5 h / -78 °C / Molecular sieve

4.2: -78 °C

5.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C

5.2: 0 - 20 °C

With pyridine; triethylsilane; phenylborondichloride; tetrabutylammoniun azide; sodium hydride; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1039/c2cc17393j

Reference yield:

: 100-39-0
benzyl bromide

: 1362022-57-8
C₂₈H₃₁N₃O₅

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

1.2: 0 - 20 °C

2.1: triethylsilane; phenylborondichloride / dichloromethane / 1.5 h / -78 °C / Molecular sieve

2.2: -78 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C

3.2: 0 - 20 °C

With triethylsilane; phenylborondichloride; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2cc17393j