N,N'-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-5-[2-(4-formylphenyl)ethenyl]isophthalamide

Base Information

• Chemical Name: N,N'-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-5-[2-(4-formylphenyl)ethenyl]isophthalamide
• CAS No.: 1239955-24-8
• Molecular Formula: C₃₉H₄₂N₆O₅
• Molecular Weight: 674.8

Synonyms:N,N'-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-5-[2-(4-formylphenyl)ethenyl]isophthalamide

Chemical Property of N,N'-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-5-[2-(4-formylphenyl)ethenyl]isophthalamide

Chemical Property:

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Technology Process of N,N'-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-5-[2-(4-formylphenyl)ethenyl]isophthalamide

There total 1 articles about N,N'-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-5-[2-(4-formylphenyl)ethenyl]isophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

N,N′-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-5-iodoisophthalamide (1094159-79-1) + 4-vinyl-benzaldehyde (1791-26-0) → N,N'-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-5-[2-(4-formylphenyl)ethenyl]isophthalamide (1239955-24-8)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenyl-arsane; triethylamine; In tetrahydrofuran; at 70 ℃; for 72h;

DOI:10.1021/ja101937w

Reference yield: 47.0%

sarcosine (107-97-1,25951-24-0) + N,N'-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-5-[2-(4-formylphenyl)ethenyl]isophthalamide (1239955-24-8) + fullerene-C60 (99685-96-8,161105-99-3,161106-00-9,111138-12-6,133318-63-5,134053-11-5,134931-35-4,134931-36-5,139703-76-7,145633-27-8,175414-73-0,175414-74-1,175414-75-2,175519-12-7,175519-13-8,175519-14-9,175519-15-0,136376-46-0,144906-37-6,144906-38-7,151767-00-9,152882-97-8,152882-98-9,152882-99-0,153062-34-1,154171-74-1,154171-75-2,154333-99-0,154334-00-6,154397-63-4,154460-59-0,199456-56-9,108739-25-9,120329-57-9,120329-58-0) → C60C2H3N(Me)C6H4CHCHC6H3(C(O)NHC5H3NNHC(O)CH2CMe3)2 (1239955-29-3)

Guidance literature:

In toluene; for 20h; Inert atmosphere; Darkness; Reflux;

DOI:10.1021/ja101937w

Reference yield: 40.0%

2-(dodecylamino)acetic acid (2274-80-8) + N,N'-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-5-[2-(4-formylphenyl)ethenyl]isophthalamide (1239955-24-8) + fullerene-C60 (99685-96-8,161105-99-3,161106-00-9,111138-12-6,133318-63-5,134053-11-5,134931-35-4,134931-36-5,139703-76-7,145633-27-8,175414-73-0,175414-74-1,175414-75-2,175519-12-7,175519-13-8,175519-14-9,175519-15-0,136376-46-0,144906-37-6,144906-38-7,151767-00-9,152882-97-8,152882-98-9,152882-99-0,153062-34-1,154171-74-1,154171-75-2,154333-99-0,154334-00-6,154397-63-4,154460-59-0,199456-56-9,108739-25-9,120329-57-9,120329-58-0) → C112H69N7O4 (1239955-30-6)

Guidance literature:

In toluene; for 18h; Inert atmosphere; Darkness; Reflux;

DOI:10.1021/ja101937w

upstream raw materials:

N,N′-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-5-iodoisophthalamide

4-vinyl-benzaldehyde

Downstream raw materials:

C₆₀C₂H₃N(Me)C₆H₄CHCHC₆H₃(C(O)NHC₅H₃NNHC(O)CH₂CMe₃)2

C₁₁₂H₆₉N₇O₄

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