N,N′-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-5-iodoisophthalamide

Base Information

Chemical Name:N,N′-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-5-iodoisophthalamide
CAS No.:1094159-79-1
Molecular Formula:C₃₀H₃₅IN₆O₄
Molecular Weight:670.55
Hs Code.:

Synonyms:N,N′-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-5-iodoisophthalamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N′-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-5-iodoisophthalamide

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Technology Process of N,N′-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-5-iodoisophthalamide

There total 5 articles about N,N′-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-5-iodoisophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 175791-94-3
5-iodoisophthalic acid dichloride

: 717110-96-8
N-(6-amino-pyridin-2-yl)-2,3-dimethyl-butyramide

: 1094159-79-1
N,N′-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-5-iodoisophthalamide

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1016/j.tet.2008.08.054

Reference yield:

: 141-86-6
2.6-diaminopyridine

: 1094159-79-1
N,N′-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-5-iodoisophthalamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 72 h / 0 - 20 °C / Inert atmosphere

2: triethylamine / tetrahydrofuran / 51 h / 0 - 20 °C

With triethylamine; In tetrahydrofuran;
DOI:10.1021/om400811z

Reference yield:

: 51839-16-8
5-iodoisophthalic acid

: 1094159-79-1
N,N′-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-5-iodoisophthalamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 6 h / Inert atmosphere; Reflux

2: triethylamine / tetrahydrofuran / 51 h / 0 - 20 °C

With thionyl chloride; triethylamine; In tetrahydrofuran;
DOI:10.1021/om400811z