1,1'-anhydro-1-C-[2',4'-bis(benzyloxy)-6'-(hydroxymethyl)-phenyl]-4,6-O-(di-tertbutylsilylidene)-3-O-triisopropylsilyl-α-D-glucopyranose

Base Information

Chemical Name:1,1'-anhydro-1-C-[2',4'-bis(benzyloxy)-6'-(hydroxymethyl)-phenyl]-4,6-O-(di-tertbutylsilylidene)-3-O-triisopropylsilyl-α-D-glucopyranose
CAS No.:1392098-01-9
Molecular Formula:C₄₄H₆₄O₈Si₂
Molecular Weight:777.158
Hs Code.:

Synonyms:1,1'-anhydro-1-C-[2',4'-bis(benzyloxy)-6'-(hydroxymethyl)-phenyl]-4,6-O-(di-tertbutylsilylidene)-3-O-triisopropylsilyl-α-D-glucopyranose

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Chemical Property of 1,1'-anhydro-1-C-[2',4'-bis(benzyloxy)-6'-(hydroxymethyl)-phenyl]-4,6-O-(di-tertbutylsilylidene)-3-O-triisopropylsilyl-α-D-glucopyranose

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Technology Process of 1,1'-anhydro-1-C-[2',4'-bis(benzyloxy)-6'-(hydroxymethyl)-phenyl]-4,6-O-(di-tertbutylsilylidene)-3-O-triisopropylsilyl-α-D-glucopyranose

There total 21 articles about 1,1'-anhydro-1-C-[2',4'-bis(benzyloxy)-6'-(hydroxymethyl)-phenyl]-4,6-O-(di-tertbutylsilylidene)-3-O-triisopropylsilyl-α-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1392097-98-1
2-[1,5-anhydro-2-deoxy-4,6-O-(di-tert-butylsilylidene)-3-O-triisopropylsilyl-D-arabinohex-1-enitol-3,5-bis(benzyloxy)]-benzyl alcohol

: 1392098-01-9
1,1'-anhydro-1-C-[2',4'-bis(benzyloxy)-6'-(hydroxymethyl)-phenyl]-4,6-O-(di-tertbutylsilylidene)-3-O-triisopropylsilyl-α-D-glucopyranose

Guidance literature:: With 3,3-dimethyldioxirane; In dichloromethane; acetone; at -78 - 20 ℃;
DOI:10.1002/chem.201304304

Reference yield:

: C₄₄H₆₄O₈Si₂

: 1392098-01-9
1,1'-anhydro-1-C-[2',4'-bis(benzyloxy)-6'-(hydroxymethyl)-phenyl]-4,6-O-(di-tertbutylsilylidene)-3-O-triisopropylsilyl-α-D-glucopyranose

Guidance literature:: With hydrogenchloride; In chloroform; water; at 20 ℃; for 1h;
DOI:10.3762/bjoc.8.82

Reference yield:

: 1392097-98-1
2-[1,5-anhydro-2-deoxy-4,6-O-(di-tert-butylsilylidene)-3-O-triisopropylsilyl-D-arabinohex-1-enitol-3,5-bis(benzyloxy)]-benzyl alcohol

: 1392098-01-9
1,1'-anhydro-1-C-[2',4'-bis(benzyloxy)-6'-(hydroxymethyl)-phenyl]-4,6-O-(di-tertbutylsilylidene)-3-O-triisopropylsilyl-α-D-glucopyranose

: 1392098-02-0
C₄₄H₆₄O₈Si₂

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.3762/bjoc.8.82