ethyl 2-(4-{[(2-tert-butoxy-2-oxoethyl){[5-methyl-2-(4-methyl phenyl)-1,3-oxazol-4-yl]methyl}amino]methyl}-2,6-dimethylphenoxy)-2-methylpropanoate

Base Information

• Chemical Name: ethyl 2-(4-{[(2-tert-butoxy-2-oxoethyl){[5-methyl-2-(4-methyl phenyl)-1,3-oxazol-4-yl]methyl}amino]methyl}-2,6-dimethylphenoxy)-2-methylpropanoate
• CAS No.: 866641-17-0
• Molecular Formula: C₃₃H₄₄N₂O₆
• Molecular Weight: 564.722

Synonyms:ethyl 2-(4-{[(2-tert-butoxy-2-oxoethyl){[5-methyl-2-(4-methyl phenyl)-1,3-oxazol-4-yl]methyl}amino]methyl}-2,6-dimethylphenoxy)-2-methylpropanoate

Chemical Property of ethyl 2-(4-{[(2-tert-butoxy-2-oxoethyl){[5-methyl-2-(4-methyl phenyl)-1,3-oxazol-4-yl]methyl}amino]methyl}-2,6-dimethylphenoxy)-2-methylpropanoate

Chemical Property:

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Technology Process of ethyl 2-(4-{[(2-tert-butoxy-2-oxoethyl){[5-methyl-2-(4-methyl phenyl)-1,3-oxazol-4-yl]methyl}amino]methyl}-2,6-dimethylphenoxy)-2-methylpropanoate

There total 2 articles about ethyl 2-(4-{[(2-tert-butoxy-2-oxoethyl){[5-methyl-2-(4-methyl phenyl)-1,3-oxazol-4-yl]methyl}amino]methyl}-2,6-dimethylphenoxy)-2-methylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

ethyl 2-(4-{[(2-tert-butoxy-2-oxoethyl)amino]methyl}-2,6-dimethylphenoxy)-2-methylpropanoate (866640-84-8) + [5-Methyl-2-(4-methylphenyl)-4-oxazolyl]methyl Chloride (137090-44-9) → ethyl 2-(4-{[(2-tert-butoxy-2-oxoethyl){[5-methyl-2-(4-methyl phenyl)-1,3-oxazol-4-yl]methyl}amino]methyl}-2,6-dimethylphenoxy)-2-methylpropanoate (866641-17-0)

Guidance literature:

With potassium carbonate; In acetonitrile; for 2h; Reflux;

DOI:10.1248/cpb.c15-00221

Reference yield:

ethyl 2-[4-({(2-tert-butoxy-2-oxoethyl)[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methyl]amino}methyl)-2,6-dimethylphenoxy]-2-methylpropanoate (866640-85-9) + [5-Methyl-2-(4-methylphenyl)-4-oxazolyl]methyl Chloride (137090-44-9) → ethyl 2-(4-{[(2-tert-butoxy-2-oxoethyl){[5-methyl-2-(4-methyl phenyl)-1,3-oxazol-4-yl]methyl}amino]methyl}-2,6-dimethylphenoxy)-2-methylpropanoate (866641-17-0)

Guidance literature:

With potassium carbonate; In acetonitrile; at 50 - 70 ℃; for 96h;

Reference yield:

ethyl 2-(4-{[(2-tert-butoxy-2-oxoethyl){[5-methyl-2-(4-methyl phenyl)-1,3-oxazol-4-yl]methyl}amino]methyl}-2,6-dimethylphenoxy)-2-methylpropanoate (866641-17-0) → 2-[4-[[carboxymethyl-(5-methyl-2-p-tolyloxazol-4-ylmethyl)amino]methyl]-2,6-dimethylphenoxy]-2-methylpropanoic acid ethyl ester (866641-18-1)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; dichloromethane; at 20 ℃; for 48h;

upstream raw materials:

ethyl 2-[4-({(2-tert-butoxy-2-oxoethyl)[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methyl]amino}methyl)-2,6-dimethylphenoxy]-2-methylpropanoate

[5-Methyl-2-(4-methylphenyl)-4-oxazolyl]methyl Chloride

ethyl 2-(4-{[(2-tert-butoxy-2-oxoethyl)amino]methyl}-2,6-dimethylphenoxy)-2-methylpropanoate

Downstream raw materials:

2-[4-[[carboxymethyl-(5-methyl-2-p-tolyloxazol-4-ylmethyl)amino]methyl]-2,6-dimethylphenoxy]-2-methylpropanoic acid ethyl ester

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