C₂₂H₂₄O₅

Base Information

• Chemical Name: C₂₂H₂₄O₅
• CAS No.: 109421-03-6
• Molecular Formula: C₂₂H₂₄O₅
• Molecular Weight: 368.43
• Mol file: 109421-03-6.mol

Synonyms:C₂₂H₂₄O₅

Chemical Property of C₂₂H₂₄O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₂₄O₅

There total 13 articles about C₂₂H₂₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

C26H32O6 → C22H24O5 (109421-03-6)

Guidance literature:

With periodic acid; In methanol; water; at 25 - 30 ℃;

DOI:10.1039/c39860001352

Reference yield:

benzoyl chloride (98-88-4) → C22H24O5 (109421-03-6)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine

2: 1.) O₃ 2.) Me₂S / 2.) MeOH

With pyridine; dimethylsulfide; ozone;

DOI:10.1271/bbb1961.47.449

Reference yield:

(E)-1-iodooct-1-en-3-ol (39178-65-9) → C22H24O5 (109421-03-6)

Guidance literature:

Multi-step reaction with 6 steps

1: tBuOOH, Ti(OiPr)4, D-(-)-diisopropyl tartrate / CH₂Cl₂

2: 100 percent / Ni(dppp)Cl₂ / diethyl ether / 3 h / Ambient temperature; addition at 0 deg C

3: 75 percent / tBuOOH, Ti(OiPr)4, L-(+)-diisopropyl tartrate, molecular sieves 4A / CH₂Cl₂ / 20 h / -20 °C

4: 93 percent / ⁿBu₄NF / tetrahydrofuran / 0.5 h / 0 °C

5: pyridine / Ambient temperature

6: 1.) O₃, 2.) Me₂S / 1.) MeOH, -78 deg C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; dimethylsulfide; L-(+)-diisopropyl tartrate; 4 A molecular sieve; tetrabutyl ammonium fluoride; D-(-)-diisopropyl tartrate; ozone; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); In tetrahydrofuran; pyridine; diethyl ether; dichloromethane;

DOI:10.1016/S0040-4039(00)80846-1

upstream raw materials:

benzoyl chloride

monilidiol

(1S,2S)-1-((R)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-heptane-1,2-diol

(1S,2S)-1-((R)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-1-(2-ethoxy-ethoxy)-heptan-2-ol

Downstream raw materials:

C₂₂H₂₆O₅