Technology Process of 9-hypoxanthine
There total 4 articles about 9-hypoxanthine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
acetic anhydride;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) HBr / 1) acetic acid, 4 h, reflux; 2) DMF, 2 h, reflux
2: 1.) hydrazine hydrate, 2.) hydrochloric acid / 1) ethanol, reflux, 10 min; 2) ethanol, reflux, 15 min
3: acetonitrile / 0.25 h / Heating
4: 96 percent / acetic anhydride / Ambient temperature
With
hydrogenchloride; hydrogen bromide; acetic anhydride; hydrazine hydrate;
In
acetonitrile;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: acetonitrile / 0.25 h / Heating
2: 96 percent / acetic anhydride / Ambient temperature
With
acetic anhydride;
In
acetonitrile;