trans-2-cyclohexanol

Base Information

• Chemical Name: trans-2-cyclohexanol
• CAS No.: 83196-12-7
• Molecular Formula: C₉H₁₆N₂O
• Molecular Weight: 168.239

Synonyms:trans-2-cyclohexanol

Chemical Property of trans-2-cyclohexanol

Chemical Property:

Purity/Quality:

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Technology Process of trans-2-cyclohexanol

There total 4 articles about trans-2-cyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + (1R,2R)-trans-2-(N-methyl)amino-1-cyclohexanol (21651-83-2) + potassium cyanide (151-50-8) → [((1R,2R)-2-Hydroxy-cyclohexyl)-methyl-amino]-acetonitrile (83196-12-7)

Guidance literature:

With hydrogenchloride; for 12h;

DOI:10.1016/S0040-4039(00)87446-8

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + rac-trans-2-methylamino-cyclohexanol (20431-81-6) + potassium cyanide (151-50-8) → trans-2-cyclohexanol (83196-12-7)

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1021/jo00168a006

Reference yield:

sodium cyanide (143-33-9,25596-52-5) + Sodium; [((1R,2R)-2-hydroxy-cyclohexyl)-methyl-amino]-methanesulfonate → trans-2-cyclohexanol (83196-12-7)

Guidance literature:

upstream raw materials:

formaldehyd

(1R,2R)-trans-2-(N-methyl)amino-1-cyclohexanol

potassium cyanide

sodium cyanide

Downstream raw materials:

cis-3a-phenyl-4-oxo-decahydrocycloheptapyrrole

{[(1R,2R)-2-Hydroxy-2-(1-phenyl-vinyl)-cyclohexyl]-methyl-amino}-acetonitrile

cis-2--1-(1-phenylethenyl)cyclohexanol

1-Methyl-cis-3a-phenyl-4-oxodecahydrocycloheptapyrrole

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