5-amino>methyl>-N-<(phenylmethoxy)carbonyl>amino>pentan-1-ol

Base Information

• Chemical Name: 5-amino>methyl>-N-<(phenylmethoxy)carbonyl>amino>pentan-1-ol
• CAS No.: 150252-73-6
• Molecular Formula: C₂₂H₂₇N₃O₅
• Molecular Weight: 413.473

Synonyms:5-amino>methyl>-N-<(phenylmethoxy)carbonyl>amino>pentan-1-ol

Chemical Property of 5-amino>methyl>-N-<(phenylmethoxy)carbonyl>amino>pentan-1-ol

Chemical Property:

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Technology Process of 5-amino>methyl>-N-<(phenylmethoxy)carbonyl>amino>pentan-1-ol

There total 3 articles about 5-amino>methyl>-N-<(phenylmethoxy)carbonyl>amino>pentan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-hydroxypentylamine (2508-29-4) → 5-amino>methyl>-N-<(phenylmethoxy)carbonyl>amino>pentan-1-ol (150252-73-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) MeOH, reflux, 2 d, 2.) 1,2-dichloroethane, 50 deg C, 1 h

2: 1.) Me₃SiCl, DIPEA, 2.) DIPEA / 1.) 1,2-dichloroethane, 40 deg C, 2 h, 2.) a) 0 deg C, 20 min, b) room temperature, 4 h

With chloro-trimethyl-silane; N-ethyl-N,N-diisopropylamine;

DOI:10.1021/jo00067a014

Reference yield:

sodium tosylate (657-84-1) → 5-amino>methyl>-N-<(phenylmethoxy)carbonyl>amino>pentan-1-ol (150252-73-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) MeOH, reflux, 2 d, 2.) 1,2-dichloroethane, 50 deg C, 1 h

2: 1.) Me₃SiCl, DIPEA, 2.) DIPEA / 1.) 1,2-dichloroethane, 40 deg C, 2 h, 2.) a) 0 deg C, 20 min, b) room temperature, 4 h

With chloro-trimethyl-silane; N-ethyl-N,N-diisopropylamine;

DOI:10.1021/jo00067a014

Reference yield:

benzyl chloroformate (501-53-1,94274-21-2) + (5-hydroxypentyl)guanidinium toluenesulfonate → 5-amino>methyl>-N-<(phenylmethoxy)carbonyl>amino>pentan-1-ol (150252-73-6)

Guidance literature:

With chloro-trimethyl-silane; N-ethyl-N,N-diisopropylamine; Yield given. Multistep reaction; 1.) 1,2-dichloroethane, 40 deg C, 2 h, 2.) a) 0 deg C, 20 min, b) room temperature, 4 h;

DOI:10.1021/jo00067a014

upstream raw materials:

benzyl chloroformate

5-hydroxypentylamine

sodium tosylate

Downstream raw materials:

N¹,N²-bis(benzyloxycarbonyl)-N¹-(5-iodopentyl)guanidine

N¹,N²-bis(benzyloxycarbonyl)-N¹-(5-[(methanesulfonyl)oxy]pentyl)guanidine

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